Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
NYC-WTC_000018664–000018683Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30907.D Vial: 43 Acq On 2 Jan 2002 5:37 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T. 14.31 2.27 ug/1 567708 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, 2, -bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 38 3 N- (Trifluoroacet yl)-0,0',0’'-tris(t 481 C19H34F3NO4Si3 000000-00-0 38 4 N-(Trifluorapfetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 38 Abundance Scan 1009 (14.310 min): 30907.D (-) m/z 72.95 100.00% 73
5000 267 355 ■ ■ i ■ ■ • ■ i • ■ ‘ ■ I ■ ' 1 • i 1 • ■ ‘ i 45 14.00 14.20 14.40 14.60 108 133154 193 223 ,293 323 | ■ 1 H , • ■ i ■ * ■' • r f i ■> Ap *.* frs"i >■ । *■! I I I | I I 1 I | I I m/z " 34.02% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 m/z 355.05 25.50% 323 miz-> 02 50 100 150 200 250 300 350 400 450 Abundance #73978: Benzoic acid, 2.5-bis(trimethylsiloxy)- trimethyls 73 355 TddnnnBBBBBdB/B/d/BnB] 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.29% 45
I ■ ■ i 147 179 223 267 .... T miz-> 50 100 150 200 250 400 300 350 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(Mmethylsilyl)no 73 14.00 14.20 14.40 14.60 1 355 m/z 268.00 8.97% 5000
45 I, 126147 193 265 376 481 * • I > < j* 1* i*| i > i H > i i > । t i it । i i **1411 4 * t-t—[—r-r-r-T miz-> 50 100 150 200 250 300 350 400 450 14.00 14.20 14.40 14.60′11
30907.D GCMS1126.M Fri Jan 25 11:35:34 2002 Page 3
NYC-WTC_000018673
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NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder