Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
NYC-WTC_000018664–000018683Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30907.D Vial: 43 Acq On 2 Jan 2002 5:37 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclohexasiloxane, dodecamethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.46 4.30 ug/1 1076710 Naphthalene-d8 15.28
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, decamethyl- 444 C12H3606Si6 000540-97-6 45 2 2H-1,4-Benzodiazep n-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 4 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 Abundance Scan 1352 (17.458 min): 30907.D (-) m/ Z 73.00 100.00%| I 73
5000 341
45 147 429 17.20 17.40 17.60 17.80
miz-> mt 117 T mmmmT [ 179.207225 251 281 3114.4. 397.., .h, 40 60 80 100120140160180200220240260280300320340360380400420'1' m/z 341.00 32.60% Abundance #56711: Cyclohexasiloxane, dodecamethyl- 73 341
5000 429 T — 1tis 17.20 17.40 17.60 17.80 147 ; 1 m/z 147.00 14.82 .... .. ......................... ..... . ............. .... miz-> 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380400420 ‘ ‘ Abundance• #48337:2H-1.4-Benzodiazepin-2-one, 7-chioro-1 3-dinydro-5- 73 341 1 1 1 1 I ■ ‘ ‘ ■ I ' • TT j 1 1 1 1 | I > 1 17.20 17.40 17.60 17.80 5000 m/z 325.0,0 11.43 45 91 ! ..... .. 116. 146 ...... 227. 269 .. 315 ■ .......... m/z-> 40 60 80 100 120140160180 200 220 240 260 280 300 320 340 360 380 400 420 ‘ Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyi- 73 239 17.20 17.40 17.60 17.80 m/z 342.00 10.97 342 5000
45 133 211 - miz—> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30907.D GCMS1126.M Fri Jan 25 11:35:38 2002 Page 4
NYC-WTC_000018674
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NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder