NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\ 1\DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 5 Cyclohexasiloxane, dodecamethy Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.46 2.51 ug/1 794551 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 38
2 1,1,1,5,7^7^7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 22
3 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
4 Silane [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
Abundance Scan 1352 (17.458 min): 30605.D (-) m/z 73.00 100.00%
73
5000
341
147 429 17.20 17.40 17.60 17.80
45 117 | 179 207 251 281 311 L L T"OC"BB89080847r
- , mpnpmngmm 397 1
m/z 341.0.0 33.21%
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #56711: Cyclohexasiloxane, dodecamethyl-
73
341
429
5000
17.20 17.40 17.60 17.80
147 m/z 147.Q0 14.39%
h 1111 n > 11
117 l 297
।।।H ।. 1. H।।।
267
। < 11. ।
311 । TTTTTTTTTT
miz-> 40 60 80 100120140160180200220240260280300320340360380400420
■Abundance #56714:1.1.1.5.7.7,7-Heptamethyl-3.3-bis(trimethylsiloxy)t
73
147 17.20 17.40 17.60 17.80
5000 267 m/z 325.00 11.50%
355 429
45 207
!
(‘444k mmmmmmmmmmmmmmmmmmmmmptm popuanpaaspanpusophe
Wz-> 40 60 80 100120140160180200220240260280300320340360380400420
Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5-
73 341 17.20 17.40 17.60 17.80
m/z 342.00 10.86%
5000
45
91 !
i 1 116 146
mmmmmmmpTpT 227 269 315 I TURDTTg
miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30605.D GCMS1126.M Wed Jan 23 08:28:50 2002 Page 5
NYC-WTC_000018205
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