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GCMS analysis log for sample AD30605, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.

NYC-WTC_000018194–000018213

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018204
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 1.85 ug/1 584627 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzenee anamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 3 3,4-Dihy•droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Ben: ic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 33 Abundance Scan 1009 (14.310 min): 30605.D (-) m/z 73.0p 100.00% 73

5000 267 355 *1 1 4 4 14 4 a f I 1 ‘I 1 T ! 45 t 89 108 133 154 177 193208223 251 14.00 14.20 14.40 14.60 mH 1192441* T r*7 tTmrrrrmrri ITnamir ..293,323339, .. m/z 267.op 36.31% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 ' ' ' m/z 355.05 26.23% 191207 251 I 323339 '1111' ''I'1 ” I'11 T1—m01150011001090—00000120muuOmuus T m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanarine, N-[(pentafluorophenyl)methylene] : 73

14.00 14.20 14.40 14.60 5000 m/z 268.00 9.72% 267 44 1. 4..... 151 179194299 250 miz-> 40 60 TO 100 120 140 160 180 200 220 240 260 280 '366' 320 340 360 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- ‘4** ' 1 1 ' > 1 1 I 73 14.00 14.20 14.40 14.60 m/z 356.0 9.17% 5000 267 179 356 45 147 209 237 312 341 — 1‘00011—0—7m0pTmnmf .. (..., ।. rn । > 11111 ri 111111| rf m 11 16mOBmB—BnBn—p8nn/n m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60

30605.D GCMS1126.M Wed Jan 23 08:28:44 2002 Page 4

NYC-WTC_000018204

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NYC-WTC_000018204Source: NYC Law Department, mirrored locally

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