NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\DEC3101\30605.D Vial: 30
Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS
Sample gems scan 12/19 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 1.85 ug/1 584627 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72
2 Benzenee anamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38
3 3,4-Dihy•droxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38
4 Ben: ic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 33
Abundance Scan 1009 (14.310 min): 30605.D (-) m/z 73.0p 100.00%
73
5000
267
355
*1 1 4 4 14 4 a f I 1 ‘I 1 T !
45 t 89 108 133 154 177 193208223 251 14.00 14.20 14.40 14.60
mH 1192441* T r*7 tTmrrrrmrri ITnamir ..293,323339, .. m/z 267.op 36.31%
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
14.00 14.20 14.40 14.60 ' ' '
m/z 355.05 26.23%
191207 251 I 323339
'1111' ''I'1 ” I'11 T1—m01150011001090—00000120muuOmuus T
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #74573: Benzeneethanarine, N-[(pentafluorophenyl)methylene]
: 73
14.00 14.20 14.40 14.60
5000 m/z 268.00 9.72%
267
44
1. 4..... 151 179194299 250
miz-> 40 60 TO 100 120 140 160 180 200 220 240 260 280 '366' 320 340 360
Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- ‘4** ' 1 1 ' > 1 1 I
73 14.00 14.20 14.40 14.60
m/z 356.0 9.17%
5000 267
179
356
45 147
209 237 312 341 —
1‘00011—0—7m0pTmnmf
.. (..., ।. rn । > 11111 ri 111111| rf m 11 16mOBmB—BnBn—p8nn/n
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
30605.D GCMS1126.M Wed Jan 23 08:28:44 2002 Page 4
NYC-WTC_000018204
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