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GCMS analysis results for sample AD30984, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.

NYC-WTC_000018248–000018261

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018257
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30984.D Vial: 38 Acq On 2 Jan 2002 12:47 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 14.31 2.56 ug/1 945584 Naphthalene-d8 15.27 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H32O3Si3 068595-79-9 43 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 N-(Trjzfluoroacetyl)-0,0',0' 1-tris (t 481 C19H34F3NO4Si3 000000-00-0 37 Abundance Scan 1009 (14.310 min): 30984.D (-) m/z 73.00 1 00.00% 73

5000 267 355 45 14.00 14.20 14.40 14.60

miz-> — ++129223 . 99 125 154 193 223 ■ ■ I • **4 I • 100 150 200 250 300 350 400 450 500 550 1 I ‘ ‘ • i ' > m/z 267.00 36.45% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 T T i ■ • • ■ । ■11 14.00 14.20 14.40 14.60 m/z 355.05 28.10% 207 323 m/z-> 50 100 150 200 250 300 350 400 450 500 550 ′ Abundance #4 9863: 3 - 4-Di hydroxy benzyl a cohol, tris(trimethyisi lyl- 73 ‘ ■ i 1 ■ • • i ■ 1 ■ ■ I ' 1 1 ' i ' 1 14.00 14.20 14.40 14.60 267 5000 179 tn/z " 9.97% 356 45 147 209 237, 312 > । * • ‘ * । * ^ * * i 1 ‘ • 1 । • * * < । » > ' * । * * » > । j * * * । < 1 1 * । * 1 miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyi)methylene] ’ I**’’I’’’’14**11+*’I 73 355 14.00 14.20 14.40 14.60 . - - 9.27% 5000

45 I 208 251 281 386 458 548 • * i • • • ■ i • • ■ • । ■ • • ■ । • ' 1 t k ' l ■i*' ' I’A ■ 111441**1 ■ • i ■ ■ • ■ i 1 ■ ' ■ I 1 1 1 1 1 1 ' ' 1 I m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.00 14.20 14.40 14.60

30984.D GCMS1126.M Wed Jan 23 08:53:30 2002 Page 3

NYC-WTC_000018257

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NYC-WTC_000018257Source: NYC Law Department, mirrored locally

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