GCMS analysis results for sample AD30010, Jan 2002

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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30010 conducted on January 9, 2002.

NYC-WTC_000016881–000016890

Folder label: “GCMS X 12/12/01 A 12/20/01”

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NYC 9/11 Public Portal Document

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Data File C: \HPCHEM\ 1 \DATA\ JAN0 302\30010.D Vial: 41 Acq On 5 Jan 2002 1:29 am Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.17 0.51 ug/1 144521 Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual I Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N- (Trifluoroacetyl) -0,0' ,0 ’’-tris(t 481 C19H34F3N04Si3 000000-00-0 43 3 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 Abundance Scan 994 (14.166 min): 30010.D (-) m/z 73.0,0 100.00% 73

5000 267 355 1 !id,200/0//d.n//0/0/0/2/0/8.t.k)T

45 — . , । 125 i 154 193 237, 323 [..... 13.80 14.00 14.20 14.40 *er+Aj*i i-1 ‘i f 144 । m/z 267.00 33.76% m/z~> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 13.80 14.00 14.20 14.40 m/z 355.05 22.32%

m/Z-> ■ 1 । ■ ■ 50 2 .323, I........................... 100 150 200 250 300 350 400 450 500 550 Abundance #58325' N-(Trifluproacetyh)-0.0‘,0"-tris(trmethylsilyl)no 73 • i ■ ‘ 11 ‘1<p•••।■ • i • ■ • ■ । 355 13.80 14.00 14.20 14.40 5000 m/z 267.90 9.10%

45 1 I 120147 193 265 481 ‘ I*‘**I*‘‘‘1***4I***‘I1‘ ‘1**[****I**[***‘11*‘‘I‘* m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] ■ i ■ ' ■ ■ i 1 ' • 1 i ■ ■ ' ‘ i ■ 73 355 13.80 14.00 14.20 14.40 m/z 356.0 8.32% 5000

m/z—> 45 ... 50 100 208 251 281 386 458 FI’l r j’sssfahi 1 1 ' 1 ' P . i , । » i > , । « । > * । । < i i । । , 150 200 250 300 350 400 450 500 548 550 m 13.80 14.00 14.20 14.40

30010.D GCMS1126.M Mon Jan 07 11:45:23 2002 Page 2

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