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GCMS analysis results for sample AD31633, February 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD31633 conducted on February 11, 2002.

NYC-WTC_000049713–000049722

Folder label: “GCMS X 1/2/02 A 1/3 - 1/4/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0302\31633.D Vial: 40 Acq On 5 Jan 2002 12:31 am Operator: 209 GALOS Sample gems scan l/2a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.17 0.42 ug/1 117190 Naphthalene-d8 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N- (Trifluoroa etyl)-O,O’,O»’-tris(t 481 C19H34F3NO4Si3 000000-00-0 47 3 Benzeneethanal line, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 47 4 3,4-Dihydrozybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 Abundance 994... Scan - (14.166 . ’min): * 31633.D (-) m/z 73.00 100.00% 73

5000- 267 355 -PPI r■ i1,1 ’ ri 45 323 [ 13.80 14.00 14.20 14.40 — . 108133 162.193,223 +.4 m/z 267.00 30.77% 300**11* 11 | 1 * * ' । * * * » । ■ > > » j ’ m/z~> 50 ioo 150 200 250 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 • i k • i ■ 1 1 ■ i ‘ 1 ■ ■ i ‘ 1 ■ 1 i 1 13.80 14.00 14.20 14.40 m/z 355-05 21.30% 207 1 । 323 • • ■ i ■ 1 i 1 m/z-> 50 100 150 200 250 300 350 400 ' ‘ 450 “ 500 550 Abundance #58325: N-(Trifluoroacetyl)-0.O‘,0"-tris(tnmethylsilyl)no 73 TT 355 13.80 14.00 14.20 14.40 5000 m/z 356.05 9.70%

45 i 120147 193 265 481 70029—manmTamamtrnu —ui—ruukuriir T-j-r-r-r-TT-r-r-r-r-j-r m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-K(pentafluoropheny!)methylene] ‘I T T TIT 73 355 13.80 14.00 14.20 14.40 m/z 74.0.0 8.50% 5000

45 208 251 281 386 458 548 ■ h"rii .-n . POPPT . ■ rf. H TT I l«i i >•. । i n i jn i i । i i 41** ■ • i ‘ 1 1 • i ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 13.80 14.00 14.20 14.40

31633.D GCMS1126.M Fri Feb 01 11:13:15 2002 Page 2 NYC-WTC_000049721

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NYC-WTC_000049721Source: NYC Law Department, mirrored locally

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