NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GC/MS analysis results for sample AD30909, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
NYC-WTC_000018693–000018715Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
14.31 4.02 ug/1 1099570 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 N-(Trifluoroacetyl)-0,0’,0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 3,4-Dihydr benzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 N- (Trifluq acetyl)-0,0',0”-tris(tri 495 C20H36F3NO4Si3 000000-00-0 37 Abundance L Scan 1009 (14.310 min): 30909.D (-) m/z 73.00 100.00% 73
5000 267 355 , 45 108 133154 . TInnnr L LTT 193 223 293 323 L ' 14.00 14.20 14.40 14.60 ' , *i, II 1 4 1**1 t 14 r '/' l । ■ 1 i -T m/z 267.00 35.26% m/z-> 50 100 150 200 250 300 350 400 ‘ ' 450' ' Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 14.00 14.20 14.40 14.60 m/z 355.05 26.91% .............................. 207 323 . : —I miz-> 50 100 150 200 250 300 '350' 400 450 Abundance ~ #58326: N-(T rifluoroacety)-0.0‘,0"-tris(trimethylsilyl)no 73 355 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.84%
45 i 126147 193 265 ) 376 481 1**11+411II*| miz-> 50 100 150 200 250 300 350 400 450 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73 14.00 14.20 14.40 14.60 ' m/z 267.90 9.16% 267 5000 179 356 45 147 209 237 , 312 ......................... .......... ... ■ • i ’ ■ ' ■ i ■ ' ■ ■ i ■ ‘ 1 i f1 • • i • • • ■ i' ■ • ■ i ■ • • ■ i ■ • m/z—> 50 100 150 200 250 300 350 400 450 14.00 14.20 14.40 14*60 ' '
30909.D GCMS1126.M Fri Jan 25 11:40:09 2002 Page 3
NYC-WTC_000018702
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NYC-WTC_000018702Source: NYC Law Department, mirrored locally
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