GC/MS analysis results for sample AD30933, Jan 28 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\ 1\DATA\DEC3101\30933.D Vial: 50 Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table • Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

14.31 1.11 ug/1 313164 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N-(Trifluoroacetyl)-N,O,O ',O1'-tetr 553 C22H42F3NO4S14 000000-00-0 47 3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 43 4 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 38 Abundance Scan 1009 (14.305 mln): 30933.D (-) m/z 73.00 100.00% 73

5000 267 355 45 125 154 193223 1323 ’ i [1 ■ ■ ■ I ■ ■ ■ 1 i ' ■ ■ ' i ' ' ■ ■ i ' • 14.00 14.20 14.40 14.60 ‘ ' — . .99 j i 1t It 11 r । । r,-. pi < . । .■ ........: 32.21% mlz-> 50 100 150 200 250 300I 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 T-r-j-r-m-] 5000 14.00 14.20 14.40 14.60 m/z 355.0 21.94% i 207 „ 323, : ‘ * I • ’ ‘ * I ‘ ‘ ‘ ‘ I ‘ ‘ k ‘ I • 1 ‘ ‘ I ’ ‘ ‘ I •0Tmma/Bndm0/n—B— miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoracety)-N,O O‘,0"-tetrakis(trimethylsi 73

355 14.00 14.20 14.40 14.60 5000 m/z 74.0,0 8.61%

45 147 193 267 I ............... 538 ■ ' i b ■ I • ‘ ■ i 1 • 1 ■ i 1 ■ ■ ■ i • ■ 1 ■ i ‘ miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #49868:3,4-Dlhydroxybenzyl alcohol,tris(trimethylsilyl) — 73 14.00 14.20 14.40 14.60 m/z 267.90 7.82% 5000 267 179 356 45 147 ... 209 237, 312 ■ i ■ ■ • ■ i • ■ ■ i ■ • ■ ( i • • ■ ■ i ■ • • ' i ' 1 ‘ ' i ■ 1 • ' i ■ 1 ' 1 i ■ ' • ■ i 1' 1 • i • • ■ ‘ i • ■ ‘ 1 I m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.00 14.20 14.40 14.60

30933.D GCMS1126.M Fri Jan 25 11:43:18 2002 Page 2

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