Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
NYC-WTC_000018716–000018732Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30933.D Vial: 50 Acq On 2 Jan 2002 2:22 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 1.89 ug/1 534649 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 35 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N2OS1 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H3003Si3 017864-23-2 9 4 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 8 Abundance Scan 1352 (17.454 min): 30933.D (-) m/z 73.0,0 100.00% 73
5000 341 147 17.20 17.40 17.60 17.80 45 mz-> mH km mmmmTmmmmpm 117 L 179.207 251 281 311 L | 397 429 rn/z 341.00 27.94% 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylslloxy)t 73 147 5000 267 ‘*‘I‘21*1*I*I* 355 429 17.20 17.40 17.60 17.80 45 207 1 m/z 147.00 14.05% mmmmmmmmmmkmmmmmmmadpmmmmmt m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one. 7-chloro-1.3-dihydro-5- 73 341
17.20 17.40 17.60 17.80 5000 m/z 325.00 9.52% 45 ' 91 i ............................................................................................................... ............ m/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380400420" Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- *‘+***I**‘I‘*I* 73 239 17.20 17.40 17.60 17.80 m/z 342.00 9.23% 342 5000
45 133 211 <>>। 11 > i A1 j 1111 ] i t < < j 11 > 11 IT 1111 >) > 11111' । > i i > । > i 11 TTT 1111JI IT J' | IUBsbabgBaasat— Fri i I j I'l I > ] J J -n-p- 1 1 I > । । i ; । । miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30933.D GCMS1126.M Fri Jan 25 11:43:23 2002 Page 3
NYC-WTC_000018725
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NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
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NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
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NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder