Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
NYC-WTC_000018754–000018774Folder label: “GCMS X 12/19/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30935.D Vial: 48 Acq On 2 Jan 2002 11:27 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.45 3.46 ug/1 1126590 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 25 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 12 4 3-Trimethylsilylpxystearic acid, tr 444 C24H52O3Si2 000000-00-0 9 Abundance Scan 1352 (17.454 min): 30935.D (-) m/ z 73.0,0 100.00% 73
5000 341 147 17.20 17.40 17.60 17.80 ‘ miz-> mhmm 45 117 | 179 207225 251 281 311 . 1 429 397..... L p i ih nf i f rhi III n rYgrri girju fn phi grin pamappaaspaniy —OUU-O—B13T11" 40 60 80 100120140160180200220240260280300320340360380400420 m/z 341.00 29.27% Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trlmethylsiloxy)t 73 147 5000 267 T T 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 14.31%
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundances #48337: 2H-1,4-Benzodiazepin-2-one, 7-chioro-1.3-dihydro 5- 73 341 i i i t B n i । j' i" 7 r । h n TA788 t ' 17.20 17.40 17.60 17.80 5000 m/z 342.00 10.24% 45 91 i 116 146 227 269 315 ; m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 * Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 1100—mT1—r 73 17.20 17.40 17.60 17.80 239 m/z 325.00 9.44% 5000 342
45 | 133 179 211 *‘I**I*-1*4*114* miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400420 * 17.20 17.40 17.60 17.80
30935.D GCMS1126.M Fri Jan 25 11:50:29 2002 Page 4
NYC-WTC_000018764
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NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018576
Single-page document containing GCMS data or metadata associated with the WTC site in early January 2002.
Filed in the same folder
NYC-WTC_000018577
Laboratory log sheet detailing Method 508 extraction and analysis parameters for samples processed in December 2001.
Filed in the same folder
NYC-WTC_000018579
Laboratory report documenting GCMS calibration data for sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018583
Laboratory report documenting GCMS reference analysis of sample AD30705 conducted on January 2, 2002.
Filed in the same folder
NYC-WTC_000018588
Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
Filed in the same folder