GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
NYC-WTC_000036842–000036859Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************** ** ************* Peak Number 7 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
17.30 0.80 ug/1 455925 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5, 7/7, 7-Heptamethyl-3,3-bis (t 444 C13H40O5Si6 038147-00-1' 25 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane/; [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 12 4 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 000540-97-6 10 Abundance Scan 1335 (17.303 min): 29670.D (-) m/ z 73.00 100.00% 73
5000- 341 / V । r. .1 । ILT 147 429 17.00 17.20 17.40 17.60 45 117 . [ 179 . 207225 251269 miz-> m r " 'i DTg ETittn I > TITTTTTTTpo 311 [ TTTT ....... 40 60 80 100120140160180200220240 260280300 320 340360 380400420 ....... - •1'1 r111 r1111'1" i'1111 m/ Z 341.00 25.76% Abundance #56714: 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73
5000 147 267 ....... A 17.00 17.20 17.40 17.60 355 429 45 207 m/z 147.00 12.97% .... .. LL.. Ti..„,i___ 4. - m/z--> 40 60 80 100120140160180200 220 240 260 280 300 320 340 360 380 400 420 Abundance #48337; 2H-1,4-Benzodiazepin-2-one. 7-chlor-1,3-dihydro-5- 73 341 I / TII IT 17.00 17.20 17.40 17.60 5000- m/ z 325.00 8.91% 45 91 V | 116 146 227 269 3154 f i" " r ■1 ■ i TTTT T‘ TTT TCIUUTT ’ I' ’' • I'" • I" " I p- m/z-> 40 60 80 100120140160180 200220 240260 280 300 320 340 360 380400420 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- / r 73 17.00 17.20 17.40 17.60 m/z 342.00 8.77% 239 5000- 342
45 . I..... 133, 179 211 YTTrp-rrTJTTTTpTTTpT ■ • i"" r'' ■ ■ i" "I ""i■ i _.................................................. I I I I | I I I t | I 4 TTTT < . ! | H I I |T * 1 . | i H l !. . < . | . . » . | < til | I ............I I I I < I I t t I I t t I
m/z-> 40 60 80 100120140160180 200220240 260280300 320 340360380400420 17.00 17.20 17.40 17.60
29670.D GCMS1126.M Wed Jan 16 14:50:56 2002 Page 7
NYC-WTC_000036855
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder