NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\JAN0302\29670.D Vial: 15
Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS
Sample gems scan 12/7 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
Peak Number 6 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.16 0.88 ug/1 497134 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50
2 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47
3 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 46
4 Ben ic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
•Abundance Scan 993 (14.164 min): 29670.D (-) m/ z 73.00 100.00%
73
5000
267
355 . ........................................... —
45 13.80 14.00 14.20 14.40
1 , 89 108 133 154 177 193208223 251 + , 1 293 111323 339
T TIUunmnuumOOTTT TI m/ z 267.00 30.36%
miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
'Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267 \
5000 l-r
13.80 14.00 14.20 14.40
m/z 355.05 21.46%
i'11' I i• ‘ 'i
191207
' ’ ’' I' •' ’ I
251
i ‘1■' i'1' ■ i
323 339
TTTTT i ■ ■'' i
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
(Abundance #<3978: Benzoic acid, 2.5-bis(trimethylsiloxy)-, trimethyls
73
355 J
1TT ■ i * ■ ■ ■ i '
13.80 14.00 14.20 14.40
5000 m/z 74.0.0 8.67%
45
. 147 179 207 223 267282297 j 370
i' • " r • " i • ’" i • • ” r • ” TTTTTTT r ■ " i' •1' i •" ■ i ■ ■ " r ■ ■ • i" ■' i
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
'Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)-
73 13.80 14.00 14.20 14.40
m/z 356.05 8.22%
267
5000 179
356
45 147
_................
I . | ll ! > | I . I I ( I t M p i l ! |
i i
209 237 ,
ITTT । i i i . j i .7. | iYi .
312 341
, TT’T Pi | I I I l p I T‘‘‘II ........ 4.........
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40
29670.D GCMS1126.M Wed Jan 16 14:50:51 2002 Page 6
NYC-WTC_000036854
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