Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
NYC-WTC_000036831–000036841Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\29666.D Vial: 64 Acq On 3 Jan 2002 3:59 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.31 0.40 ug/1 166690 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid, ,5-bis (trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 Benzeneethana ine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 4N-(Trifluoroacetyl)-N,0,0‘,0‘ -tetr553.C22H42F3N04Si40 00000-00-0 38 Abundance Scan 1009 (14.310 min): 29666.D (-) m/z 72.95 100.00% 73
5000 267 355 .......... / i 45 14.00 14.20 14.40 14.60 103 133 154170, 191207223 251 323339 mlz-> ' m40n TT TTTT p1 f' i I ‘,r' I - BIUBuBpnnn TT m/ z 2 67.00 33.69% 60 80 100.120 140 160 180 200 220 240 260 280 300 320 340 360 ’Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 - 14.00 14.20 14.40 14.60 m/z 355.05 26.48% 191207 251 s 323339 | pi ii | » i > r । TTTTTTTTTTT i•r ■i " ■ ■ i " " i " " i1" ') ■ " ' i ■ ■ " i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73978: Benzoic acid, 2.5-bis(trimethylsiloxy)-, trimethyls 73 355 14.00 14.20 14.40 14.60 5000 m/z 356.05 9.81% 45 | 147 179 207223 267282 ' i11 ‘dT 1‘‘‘11‘111111111‘EOT"ETTTTTETT‘ETVIEVETOETLTTTTTTTETTT‘TT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 7400 1428 14.40 14*60 ' ' ' m/ z 268.00 8.77% 5000 267 44 — 151 179 209 250 i' " ' i " " r " ' i " " r ■ “ i " ’ITT " 11' ।11111111' TIIE"EIICCE-F"‘EI1°"II1‘‘I‘T ■ i ■ ■ ■ ■ i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60
29666.D GCMS1126.M Wed Jan 16 14:45:48 2002 Page 3
NYC-WTC_000036840
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000037406
Laboratory notes stating that GCMS scanning of sample AD29782 did not reveal the presence of unusual compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049734
GCMS analysis report for sample AD31642 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049762
GCMS analysis report for sample AD31640 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049723
GCMS analysis report for sample AD31632 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017958
Laboratory report documenting GCMS analysis of sample AD30489 conducted on January 24, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018983
GCMS analysis report for sample AD31135 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019004
GCMS analysis report for sample AD31130 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049713
GCMS analysis report for sample AD31633 conducted on February 11, 2002.
Similar document embedding; no shared entity or topic indexed. · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049693
GCMS blank analysis report for sample AD31586 conducted on February 11, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049851
Laboratory report showing GCMS analysis of sample AD29519 including unknown compounds and surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017097
Laboratory report detailing GCMS analysis of sample AD30486 including DDD surrogates on January 18, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049823
Laboratory report showing GCMS analysis of sample AD29292 including unknown compounds and surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder