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GCMS analysis results for sample AD29522, Jan 2002

Machine-extracted title · confidence 100%

Quality reviewed GCMS data listing surrogate compounds and retention times from January 3, 2002.

NYC-WTC_000036752–000036778

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036760
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan 2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

14.31 14.43 ug/1 9557740 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 72 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 3 Noradrenal/ne, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 37 'Abundance Scan 1009 (14.311 min): 29522.D (-) m/z 73.00 100.00%| 73

5000- 267 355 .... A......... 14.00 14.20 14.40 14.60 i 0- 45 — 108,133 154173 123 ,223 247 1 293 323 1 । 1 ■ ■ ■ ■ । ■ m/z 267.00 38.04% m/z-> 50 100 150 200 250 300 350 40G (Abundance #51266: Cyclopentasiloxane, decamethyl- i 73 355 i 5000 267 / —r-T-J-I-T-T-T-J 14.00 14.20 14.40 14.60 I m/z 355.05 30.67% 207 323 1 miz-> 50 100 150 200 250 300 350 400 Abundance #51296: Benzoic acid, 2.6-bis[(trimetliylsilyl)oxy]-. trimet 73 355 __ — ..... ................................. — 14.00 14,20 14.40 14.60 5000 m/z 356.05 10.70% 147 267 47 208 237 i 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #57357: Noradrenaline, tetra-TMS -----.............. 7)3 14.00 14.20 14.40 14.60 m/z 268.00 9.77% 5000- 102 355

45 147 1 T r 442 - ----- IT m/z- 50 100 150 200 250 300 350 400 14.00 14.20 14.40 14.60

29522.D GCMS1126.M Fri Jan 18 16:48:17 2002 Page 3

NYC-WTC_000036760

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NYC-WTC_000036760Source: NYC Law Department, mirrored locally

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