GCMS analysis results for sample AD29522, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\29522.D Vial: 63 Acq On 3 Jan.2002 3:00 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 1,5-Cyclooctadiene, (E,Z)- Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

11.84 13.08 ug/1 7000040 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Te ative ID MW MolForm CAS# Qual

1 1,5-Cyclooctadiene, (E,Z)- 108 C8H12 005259-71-2 59 2 Cyclohexene/ 4-ethenyl- 108 C8H12• 000100-40-3 47 3 1,5-Cyclooctadiene, (Z,Z)- 108 C8H12 001552-12-1 45 4 2-Pentenenitrile 81 C5H7N 013284-42-9 45 Abundance Scan 740 (11.842 min): 29522.D (-) m/ z 54.00 100.00%| 4

■ I 39 80 I 5000 107 67 92 t-t-f 11.60 11.80 12.00 12.20 TT# 1 + L ‘ i Trgrt , I। । । 151 | 207 I ,| 4 . k ‘TTTTTTT . . . . । ‘TT m/z 3 9.00 53.01% m/z-> 20 30 40 50 60 70 80 90 100110120 130 140 150160 170 180 190 200 210 Abundance #2170: 1,5-Cyclooctadiene, (E,Z)- 54

39 67 5000 79 11.60 11.80 12.00 12.20 93 m/z 80.00 50.76% T" " I || p-1 J 1 108 j ■1 •11' > " I " ■ ■ I I" " r T’TTT m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #63795: Cyclohexene, 4-ethenyl- 54 ■ । r i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ 11.60 11.80 12.00 12.20 79 5000- 39 m/ z 79.0,0 50.67% 66 27 93 1 108 ‘T p i n |THT| i” "i1" 'i ।। ।।।।।।।। n rt p . n । i iti p i i-i 1111 miz--> 20 30 40 50 60 70 80 90 100 110120130140 150160 170 180 190 200 210 Abundance! #2182: 1,5-Cyclooctadiene, (Z,Z)- P 1। । ■ ।<। ■> i 54 67 11.60। 11.80 12.00 12.20 I' i m/z 41.05 50.44% 39 5000 80

108 93 m/z-> r'1' i | l I’TT rjn rf| । ...p 11 >p 11 (pt 11 p 11 ip । n । 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 —PPmm 11.60 11.80 12.00 12.20

29522.D GCMS1126.M Fri Jan 18 16:48:12 2002 Page 2

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