GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
NYC-WTC_000036842–000036859Folder label: “GCMS X 12/7/01 A 1/2/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\JAN0302\29670.D Vial: 15 Acq On 4 Jan 2002 12:13 am Operator: 209 GALOS Sample gems scan 12/7 Inst : GC/MS 209 Mise. Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 Cyclotetrasiloxane, octamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.00 0.94 ug/1 447407 1,4-Dichlorobenzene-d4 11.53
Hit# of 5 Tenbative ID MW MolForm CAS# Qual
l Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 80 2 2-Oxo-4-phenyl-6- (4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 3 3, 6-Bis (N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 648 (10.997 min): 29670.D (-) m/z 281.00 100.00% 2(11
5000
10.60 10.80 11.00 11.20 11.40 45 59 ’1 89 103 119 112 147 165177 123207 221 235 249 265 , + m/z 2 82.00 28.91% miz—> 40 60 80 100 120 140__ 160 180 200 220 240 260 280 'Abundance #72646: Cyclotetrasiloxane, octamethyl- 281
5000- 4 10.60 10.80 11.00 11.20 11.40 265 m/ z 283.00 18.42% 45 59 73 133 177 123,207 , 235 1 I ' ■ 1 1 i ' ' 1 ' I ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 ,2-dihydropyrimi 281 ........ / \........... 10 60 10.80 11.00 11.20 11.40 5000 m/z 192.90 1 2.39%
102 123 141 175 204 247 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624: 3,6-Bis(N-dimethylamino)-9-ethylcarbazole 281 10.60 10.80 11.00 11.20 11.40 m/z 133.00 11.59% 5000 266
141 . 237 250 1
m/z--> ' I 1 • ' 1 1 ' 40 60 ■ । ■ ■ ■ 1 । 1 1 1 • । 80 100 120 | TTm 140 —.. 2082224/444 / 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 11.40
29670.D GCMS1126.M Wed Jan 16 14:50:37 2002 Page 3
NYC-WTC_000036851
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NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000036689
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036690
Laboratory results for GCMS blank analysis of sample AD29522 showing detection levels below method detection limits.
Filed in the same folder
NYC-WTC_000036695
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036703
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder
NYC-WTC_000036704
Calibration table and data for GCMS analysis of sample AD29522 listing target compounds and response factors.
Filed in the same folder