GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\JANO 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

11.00 0.30 ug/1 76278 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 43 3 2-Oxo-4-phenyl-6-4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 3,6-Bis (N-dimetyHylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance Scan 648 (10.996 mln): 27288.D (-) m/z 281.00 1 00.00% 281

5000-

45 57 73 | 87 103 119 133 147 165 179 193 297 249 225 10.60 10.80 11'00 11.20 11.40 ' ■ 11 ’ it • ■ a i M ■ I ] | 'l 'l । । 7 . > । । > . . . 1***1*4431* i , . । ." 1 , । Prr m/z 282.00 28.37% mlz~> 40 60 80 100 120 140 .160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 • i ■ ■ • ■ i ■ ■ 10.60 10.80 11.00 11.20 11.40 m/z 283.00 19.53% 73 133 | 163 ,401 177 191 207 235 249 265 1 ■ ■ i ' ■ ■ • i ■ ■ ‘ ' i • ■ ■ ' i ‘ 1 ' ' i ‘ ■ i ■ ■ • ‘ i ■ ■ • i • • • . । . i . Mz-> 40__ 60 80___ 100 120 140 160 180 200 220 240 260 280 Abundance 230042 enzens 1-nherete neylethenyi) 281 .... y....... 10.60 10.80 11.00 11.20 11.40 5000 m/z 133.0.0 13.16% _ 253 126 203 266 224 240 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi i ■ ■ ■ 1 i ' ■ ■ ■ i ' ■ i • ■ ' ■ i ■ ■ 281 10.60 10.80 11.00 11.20 11.40 m/z 192.90 12.41% 5000

W2 123 141 175 204 247 .................. ■ ‘ i • ■ ■ ■ i ' ‘ ‘ i ■ ' ‘ ' "l ‘ ‘ ’1’1111111-11111111 ■■ i'1 ■ " i' ■ " l ■11 “ “ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 11.40

27288.D GCMS1126.M Mon Feb 04 15:22:54 2002 Page 2

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