NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis summary, sample AD27288, Dec 2001
Machine-extracted title · confidence 100%GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
NYC-WTC_000016096–000016117Folder label: “GCMS X 12/26/01 A 1/15-1/16/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JANO 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
14.17 2.10 ug/1 662556 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 N-(Trifluoroacetyl )-0,0’,0’’-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 Benzoic acid, 2— (trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 4 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H32O3Si3 068595-79-9 38 Abundance Scan 994 (14.172 mln): 27288.D (-) m/ z 73.00 100.00% 73
5000 267 355
• 45 i । ‘i ■ ‘ , 108,133154 1193223 247,1 ,293 323 i 13.80 14.00 14.20 14.40 14.60 m/z 267.0.0 36.99% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 13.80 14.00 14.20 14.40 14.60 m/z 355.0,5 28.63% ' 1 i ' r1 ... 27* 323 1 m/z-> Abundance 50 100 150 200 250 300 $58328 friTniluomacetyb-000"mstt nethy 350 400 Tino 450
73 355 13.80 14.00 14.20 14.40 14.60 5000 m/z 268.00 10.01%
45 , 126147 193 265 ■ 376 481 ■ ■ । miz-> 50 100 150 200 250 300 350___ 400 450 - Abundance #72298: Benzoic add, 2-[(trimethylsilyl)oxy]-, trimethylsi 73 267 13.80 14.00 14.20 14.40 14.60 m/z 356.05 9.79 5000
135 4 on 47 ■ • i ' 1 _23 11 * I IT - m/z-> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40 14.60
27288.D GCMS1126.M Mon Feb 04 15:22:59 2002 Page 3
NYC-WTC_000016105
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