Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.
NYC-WTC_000017405–000017433Folder label: “GCMS X 12/20/01 A 1/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.17 5.82 ug/1 1925000 Naphthalene-d8 15.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Benzoic acid, 2,6-bis [ (trimethylsil 370 C16H3004Si3 003782-85-2 50 3 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4S13 000000-00-0 47 4 N-(Trifluoroacetyl)-0,0,0 1 ' - tris(t 481 C19H34F3NO4S13 00000 0-00-0 47 Abundance Scan 994 (14.166 mln): 31074.D (-) m/z 73.00 100.00% 73
5000 267 355 ----- . 451 1 108 133154 193223 .4 293 2r 11*II4 13.80 14.00 14.20 14.40 " 1 ‘ 323 L ■ 'i 1 ■ m/z 267.00 32.85 m/z~> 50 100 150 200 250 300 350 400 450 500 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 5000 267 ........ 1i ■ ■ ■ ■i■ ■ ■ / X-. ..... - 13.80 14.00 14.20 14.40 m/z 355.05 23.54% ............... 207 323 I m/z-> 50 IPO 150 ' ‘ 200 ‘ 250 ' ‘ ‘360’ 350 400 450 500 Abundance 51290: Bonzo acid 2.0-bsi(tritnemvisilylaj-, trimet 73 355 ----- 13.80 14.00 14.20 14.40 ‘ ‘ ‘ ‘ 5000 m/ z 356.0 8.64 147 267 47 208 237 । m/z-> 50 ' 100 ' ’ 150 ' ‘ '200 ' ‘ ‘256 ' 300 ‘350‘ 400 ′ 450 ‘ ' 500 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethyIsiIyI)epin 73 13.80 14.00 14.20 14.40 ‘ ‘ ‘ 355 m/z 268.00 8.34% 5000
45 _ k 1 • 1 ■ ■ ■ ......140 184 .281 1 II’IIIII 480 m/z-> 50 100 150 1 200 250 ' 300 ' ' '350 400 450 500 13.80 14.00 14.20 14.40
31074.D GCMS0103.M Wed Jan 09 12:24:42 2002 Page 7
NYC-WTC_000017419
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NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017329
Document page containing only the CCAS identifier with no readable text or specific content details visible.
Filed in the same folder
NYC-WTC_000017330
Fragmented page from a laboratory method document regarding extraction and analysis procedures for GCMS testing.
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NYC-WTC_000017334
Laboratory report documenting GCMS calibration analysis of sample AD31017 conducted on January 8, 2002, listing concentrations of various organic compounds.
Filed in the same folder
NYC-WTC_000017338
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.
Filed in the same folder
NYC-WTC_000017344
Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.
Filed in the same folder