GCMS analysis results for sample AD31074, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptane Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

12.80 0.69 ug/1 182090 1,4-Dichlorobenzene-d4 11.52

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane / 100 C7H16 000142-82-5 64 2 Undecane, 2,8-dimethyl- 184 C13H28 017301-25-6 59 3 Nonane, 3,7-dimethyl- 156 C11H24 017302-32-8 53 4 Pentanoic acid, 2-methyl-, 1-methyl 172 C10H20O2

r 057983-17-2 53 Abundance Scan 845 (12.799 mln): 31074.D (-) 57.00 1 00.00% 57 71 43 5000 85 1240' 12.60 12.80 13.00 13.20 m/z-> 20 ...... llapa 11TT 70'' 80 do ‘ 100 110 126 130' 140141 iso' 160 m/z 30__ 40... 50 60 99 71.05 112 84.99% Abundance

MN #63439: Heptane 43

5000 57 71 12.40 12.60 12.80 ‘13'00 13.20 27 m/z 43.05 68.89% 14 /Mr 85 100 ' i • ■' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ 1 ■ ■ ■ ■ 1' ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance 43 57 71 12.40 12.60 12.80 ‘13'00 13.20 5000 i/z 56.00 -44.94% 85 27 99 141 113 TT i ■ ■' ■ 1 ■ ■ ■' i ■ • ■ ■ 1 ■1 ■ ■ 1 ‘ ■ i'' m/z-> 20 ‘ ‘ 30 ‘ ‘ 40 ‘ 50 ' ‘ 60 ‘ ‘ 70 80 90 100 110 120 130 140 150 160 Abundance" #11601: Nonane, 3,7-dimethyl- 57 12.40 12.60 12.80 13.00 13.20 43 71 m/z 41.05 38.48%

/VW 5000 85

97 127 ‘ i ■11' i ‘ ■ i ■ ■ ■ ■ i' ■ PIpT TIm 1 »''i ■ ■ ■ > । ■ 11 ■ — i' ■ ■ ■ i ■ ‘ ■ i ■156 1 ■ ■ i • • m/z-> 20 30 40 50 60 70 80 90 100 110 120_130 140 150 160 12.40 12.60 12.80 13.00 13.20

31074.D GCMS0103.M Wed Jan 09 12:24:37 2002 Page 6

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