GCMS analysis comments for sample AD29466 re-analysis required, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0802\29466.D Vial: 6 Acq On 8 Jan 2002 5:14 pm Operator: 209 GALOS Sample Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Heptane Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T.

12.80 3.48 ug/1 1458800 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptane / 100 C7H16 000142-82-5 59 2 Undecane/ 2,8-dimethyl- 184 C13H28 017301-25-6 47 3 Nonane/3-methyl- 142 C10H22 005911-04-6 43 4 Nonane, 2,6-dimethyl - 156 C11H24 017302-28-2 40

N Abundance ! Scan 845 (12.804 min): 29466.D (-) m/ z 57.00 100.00% 57 71 43 5000 85 TTB TECEITLTI-CEECIII.T 12.40 12.60 12.80 13.00 13.20

m/z-> 0— 20 30 + 50, +TT +78+ 40 50 60 70 99 111'1 TH ' 80 90 100 110 +12 , J26, 141 , 155 , . 120 130 140 150 160 m/ m/zz 71.05 65.41%

MJ Abundance #63439: Heptane 43

5000- 57 . । ""‘11." , , CE—rL[L । 71 • 12.40 12.60 12.80 13.00 13.20 27 m/z 43.05 58.94% L 85 , 19....... ,...............,,,,,,,

VuWn __ L ' I ' ' ' ' I ' ' ' ' I 1 1 1 ' miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #18991: Undecane. 2,8-dimethyl- 43 57 71 12.40 12.60 12.80 13.00 13.20 5000 m/z 56.00 49.13% 85 27 141 I 1 99 113 m/z-> Abundance • i ■ ■ ■ ■ i ■ 20 30 ■ i' ' ' ‘ i ' ' ■' i' 40 50

5(7 60 70 80 90 100 110 120 130 140 150 160 #66202: Nonane, 3-methyl- I II 12.40 12.60 12.80 13.0 41.05 13.20 39.79% 43 71 5000

27 — 1 — । 1 ।1 I ।1। ।I'' _ or 112 142 +TP 1 ' ' ' I ' 1 ' ' I ’ ’11 TT ' 1 1 1 1 1 1 I 1’1’1 i । i i । i r j i ( i 11 i । • m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 12.40 12.60 12.80 13.00 13.20

29466.D GCMS0103.M Wed Jan 09 16:16:15 2002 Page 4

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