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GCMS analysis report for sample AD26392, Dec 2001

Machine-extracted title · confidence 100%

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.

NYC-WTC_000031530–000031549

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26392.D Vial: 5 Acq On : 30 Nov 2001 3:52 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Heptane, 2,3-dimethyl- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T, 5.01 1.13 ng/uL 496196 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual l Heptane,/2,3-dimethyl- 128 C9H20 003074-71-3 9 2 5-Hexe:n-2-one 98 C6H10O 000109-49-9 7 3 4-Hexen-2-one 98 C6H10O 025659-22-7 7

A 4 3,5-Hesxadien-2-ol 98 C6H10O 003280-51-1 7 Abundance Scan 19(5.013 min): 26392.D(-) m/z 43.00 100.00% 43

5000

+ I TI—I——mamRT 55 83 98 4.90 5.00 5.10 5.20 5.30 5.40 m/z 83.05 15.76% mss 10 20 30 40 50 60 70 80 90 100 110 120 13C Abundance #5152: Heptane, 2,3-dimethyl- 43

5000 I-- TTTPIILWTLTTT 4.90 5.00 5.1 5.20 5.30 5.40 57 84 m/z 55.10 14.98%

miz-> 1 10 20 30 40 15o 27 III 71 - TI3ITIIT 90 100 । 110 128 > rj-m-r[TT 120 130 60 70 80 Abundance #63206: 5-Hexen-2-one 43

4.90 5.00 5.1 5.20 5.30 5.40

AQ 5000 m/z 42.05 10.39% 55 27 49,. 71 83 98 ................... f........ miz-> 10 20 30 40 IItF i. ।. .. TIT . T TTT ।11 ।।।. 50 60 70 80 90 100 1 > 120 130 Abundance #1260: 4-Hexen-2-one T T T r 43 T 4.90 5.00 5.10 5.20 5.30 5.40 m/z41.00 9.40% 5000

55 98 29 15 I I L I i 1 I I II I I I t I I I I : I I I II I I I I II 83 ----- II

m/z—> 10 20 30 40 50 60 70 80 90 100 11 120 130 4.90 5.00 5.10 5.20 5.30 5.40 ' |1

26392.D NP112701.M Tue Dec 04 10:43:08 2001 Page 1

NYC-WTC_000031538

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NYC-WTC_000031538Source: NYC Law Department, mirrored locally

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