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GCMS Analysis Report for Sample AD26388, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26388 with a note regarding unknown compounds.

NYC-WTC_000031452–000031472

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26388.D vial: 14 Acq On : 1 Dec 2001 12:02 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexene-2,5-diol Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 5.02 1.34 ng/uL 591056 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexene-2,5-diol 116 C6H12O2 007319-23-5 25 2 5-Hexen-2-one 98 C6H10O 000109-49-9 16 3 1, 3-Oxathiolane-2-propanol, 2-methy 162 C7H14O2S 036651-30-6 9 4 Heptane, 2,3-dimethyl-___________ 128 C9H20 003074-71-3 9

/N Abundance 2 Scan 19 (5.020 min): 26388.D (-) m/z 43.00 _100.00% 43

5000

55 83 T Tr' ” IT 98 4.90 5.00 5.10 5.20 5.30 5.40 .......................... .... , 51 ITpr . . TttmuapeT m 70 m/z , 83.05 17.26% miz-> 20253035404550556065 70 75 80859095 100 105 Abundance #3285: 3-Hexene-2,5-diol 43

AC 5000 —111' • I' " ' I •''' I ‘" I''' ‘ I'' “ I' 4.90 5.00 5,10 5.20 5.30 5.40 55 83 m/z 55.10 16.24% 98 . , 61 TI—0—Truu T Dpt I li i | hi mP a| I...।>>11111111>11 111 71 mlz—> 20253035404550556065 70 75 80859095 100 105 Abundance #1291: 5-Hexen-2-one 43

4.90 5.00 5.10 5.20 5.30 5.40 5000 m/z 42.Q0 12.27% 55 27 37 1 ‘ ।1'1 * । ■11 ‘ । ■1 ■11 ‘ “ ।" Tmpt 50 —— 69 ——— 83 9 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #12808:1,3-Oxathiolane-2-propanol, 2-methyl- 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z

N 41.00 10.31% 84 5000

54 69 60 । m/z—> 4 Ipu । “ “ । ■■ ■■ i ■ ■" i mmmpn 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 I' l " • ‘ l “ 111’011 | i l J J |T

26388.D NP112701.M Tue Dec 04 10:40:19 2001 Page 1

NYC-WTC_000031458

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NYC-WTC_000031458Source: NYC Law Department, mirrored locally

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