Laboratory report documenting GCMS analysis of sample AD26677 identifying unknown compounds on December 10, 2001.
NYC-WTC_000031989–000032006Folder label: “GCMS X 11/7/01 A 12/6/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC0601\26677.D Vial: 11 Acq On 6 Dec 2001 7:17 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 1 3-Hexene-2,5-diol Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
5.01 1.11 ng/uL 310834 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Hexene-2,5 -diol 116 C6H1202 007319-23-5 45 2 4-Penten-2-one, 4-methyl- 98 C6H10O 003744-02-3 42 3 3,5-Hexadien-2-ol 98 C6H10O 003280-51-1 33 4 2-Pentanone, 3-methylene- 98 C6H10O 004359-77-7 9 Abundance 7 Scan 18 (5.010 min): 26677.D (-) m/z 43.00 100.00% 43
5000- 55 83 98
m/z-> • I ” • • I ’' ” I • 20 25 30 J THr mH . 51 35 40 45 50 55 60 65 70 75 80 85 i 69 ■ । • ■ ■ ■ । ■ 1111 ■ ‘I‘ 4 90 95 100 105 4.90 5.00 5.10 5.20 5.30 5.40 m/z , 83.05 29.19% Abundance #3285: 3-Hexene-2,5-diol 43
5000 i 1 ' I • ■' ' I ' ' ' • I ’ ' ' ' I ' ' ' ' I 4.90 5.00 5.10 5.20 5.30 5.40 55 83 m/z 55.10 27.44% 98
A I . 61 11' “ ' I' —Hmm 71 I I'1111" 11111" I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1244: 4-Penten-2-one, 4-rnethyl- 43 nr 4.90 5.00 5.10 5.20 5.30 5.40 — 5000 m/z 41.10 17.56% 83 29 39 55 98 i i ■ i ■ ■ ■ • i'1 ■11 ■ 11'11111 11''11111'' 11 ‘ l i... 1. > lb I.... 11TTTT Illi T‘T 1111111111 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1271: 3,5-Hexadien-2-ol IrTTT j i i r * | I I I i | I i i I | TTT TII t I 1 |
A I I 43 4.90 5.00 5.10 5.20 5.30 5.40 m/z 42.0.0 13.96% 5000 55 . 83 79 98
m/z- ■ i •1 ■ ■ i ■ " ■ i ■ ■ •111 • ■ ■ i ■ H 51 I
20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71 1111111111| 111 '111 +r +t T111 > 11111111111
4.90 5.00 5.10 5.20 5.30 5.40
26677.D NP112701.M Fri Dec 07 14:52:19 2001 Page 1
NYC-WTC_000031996
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NYC-WTC_000031968
Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032245
Gas chromatography-mass spectrometry analysis of sample AD26832 documenting unknown compounds with reference to comments.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032007
Laboratory report documenting GCMS analysis of sample AD26678 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032142
Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032202
Laboratory report documenting GCMS analysis of sample AD26829 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032093
Laboratory report documenting GCMS analysis of sample AD26682 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031920
Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032058
Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032343
Laboratory report for GCMS analysis of sample AD26982 completed on December 11, 2001, noting unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032182
Laboratory report documenting GCMS analysis of sample AD26828 identifying unknown compounds on December 10, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031333
Laboratory report documenting GCMS analysis of sample AD26321 with unidentified compounds detected.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000032362
Laboratory report for GCMS analysis of sample AD26983 completed on December 11, 2001, with surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031869
Illegible text on a single page from the GCMS folder covering November to December 2001.
Filed in the same folder
NYC-WTC_000031870
Index or cover sheet page for the GCMS folder covering the period from November 7 to December 6, 2001.
Filed in the same folder
NYC-WTC_000031876
Calibration table listing standards like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 for GC/MS analysis dated December 2001.
Filed in the same folder
NYC-WTC_000031889
GC/MS analysis of sample AD26538 identified other unknown compounds noted in comments section, December 10, 2001.
Filed in the same folder
NYC-WTC_000031905
Laboratory report documenting GCMS analysis of sample AD26624 identifying unknown compounds on December 10, 2001.
Filed in the same folder