GCMS analysis results sample AD26832, December 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26832.D Vial: 5 Acq On 6 Dec 2001 1:50 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexene-2,5-diol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

5.01 1.28 ng/uL 367622 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexent -2,5-diol 116 C6H1202 007319-23-5 36 2 5-Hexerr-2-one 98 C6H10O 000109-49-9 16 3 Heptane, 2,3-dimethyl- 128 C9H20 003074-71-3 9 4 3,5-Hexadien-2-ol_____________ 98 C6H10O _________ 003280-51-1 7 Abundance / Scan 18 (5.011 min): 26832.D (-) m/z 43.10 100.00% 43

5000

55 83 l * ■ > ■ i ■ ■ > ■ i ■ ■ • ■ । ■ ■ ■ ■ ।

i । miz->____ 20 ......... . 11'1111111111 30 40 — 50 60 —ZP 70 80 90 98

100 110 120 130 4.90 5.00 5.10 5.20 5.30 5.40 m/z 83.05 19.38% Abundance #3285: 3-Hexene-2,5-diol 43

5000 U‘tE-TEETTTEEETT‘"E10111IT 4.90 5.00 5.10 5.20 5.30 5.40 55 83

U m/ Z 55.10 18.75% 71 98 - —1 . । 1 ‘IF m/z-> 20 . 30 40 50 60 70 80 90 100 110 120 130 Abundance #1291: 5-Hexen-2-one 43 \A r I ■ ■‘•I'''' I ' ' ' • I i ■ ' • ■ i 4.90 5.00 5.10 5.20 5.30 5.40 5000- m/z 42,05 11.79% 55 27 98 37 69 83 I .।।. i . | > i . -11—————————— r mlz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5152: Heptane. 2,3-dimethyl- t 43 4.90 5.00 5.10 5.20 5.30 5.407 m/z 41.00 9.34% 50001

57 84 27 — 71 - 128 -- 1*1/1///———O—BO—GGOnnnn/uon m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 4.90 5.00 5.10 5.20 5.30 5.40

26832.D NP112701.M Fri Dec 07 14:55:27 2001 Page 1

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