GCMS analysis results sample AD26832, December 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC0601\26832.D Vial: 5 Acq On : 6 Dec 2001 1:50 pm Operator: GALOS Sample .: gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1-Pentanol, 4-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

5.11 1.35 ng/uL 388128 1,4-Dichlorobenzene-d4 . 11.89

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 1-Pentanol, 4-methyl- 102 C6H140 000626-89-1 33 2 Oxirane/ (1-methylethyl)- 86 C5H10O 001438-14-8 23 3 Ethane / diazo- 56 C2H4N2 001117-96-0 9 4 Cyclobutane 56 C4H8 000287-23-0 9 Abundance Scan 29 (5.112 min): 26832.D (-) m/z 41 ,10 100.00% 41 56 59

5000

45 71 4.90 5.00 5.10 5.20 5.30 5.40 5.50

m/z--> ----- + +5053 +74 r ■ ■ ■ r'" r ' " i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 m/z 56 10 78.67% Abundance #63578: 1-Pentanol, 4-methyl- " i 56 41 69 5000- Tr TTT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59 10 70.87% 45 |59 84 i ‘ ‘I i""r"'i i""r■•■i ■ i • ■■ ■ I TTI I ‘ " ■ i ■ • ■ ■ i"'' i' •' ‘ i" " I m/z-> 5 1G 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 •Abundance #721: Oxirane. (1-methylethyl)- ! 56 41 4.90 5.00 510 5.20 5.30 5.40 5.50 T 5000- m/z 42 05 67.20%

J 27 71 37 5053 ' 85 11 r ■ " i' T’TTTTTTTTTTTTTT l1 ■ ’ • I •" ’ I ■ i ■ >■ ■ i ■ r " ■ i ■ ■ ■ ■ r '11111 ■' I ■ i" " i" " i mlz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #71: Ethane, diazo- TTITOTTrT 27 4.90 5.00 5.10 5.20 5.30 5.40 5.50

A 56 m/z 43.10 58.56% 5000

14

m/z-> 5 +L .+24 5053, I'1H i" "i" " i" " i"1' I ——mmmmu"n)——ump*u*——19T 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.90 5.00 5.10 5.20 5.30 5.40 5.50

26832.D NP112701.M Fri Dec 07 14:55:29 2001 Page 2

NYC-WTC_000032254