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GCMS analysis results for sample AD26625, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26625 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031920–000031939

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031937
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File C : \HPCHEM\1\DATA\DEC0601\26625.D Vial: 8 Acq On 6 Dec 2001 4:34 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 2-Pentanol, 3-chloro-4-methyl - Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.53 1.19 ng/uL 383907 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanol, (R@ 136 3-chloto-4 -methyl- , C6H13C1O 074685-47-5 43 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 38 3 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 4 2-Pentanol, 4-methyl-___________ 102 C6H140 000108-11-2 35 Abundance Scan 620 (10.525 min): 26625.D (-) m/z 43.10 ’100.00% I 4b

5000-

57 85 IPI—* -PRT 39 10.20 10.40 10.60 10.80

m/z-> ‘ i 20 25 30 4/ +53+4 mmmmmmmmmp+ HPpm 61

35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 69 100 m/z 45.10 65.62% Abundance #6421: 2-Pentanol, 3-chloro-4-methyl-, (R@,R@)( +/-.)- 45

A) v 5000 I ' ' ' ' I 10.20 10.40 10.60 10.80 m/z 41.10 29.52% 27 69 85 76 100 i ■11r mP I''1' I - TTT rr TTTIu I' ‘' I 20 25 30 35 40 45 50 55 60 65 70 75 180 85 90 95 100 105 Abundance #1773; 2-Pentanol, 4-methyl- i 45 — — TTTTTT 10.20 10.40 10.60 10.80 5000 - m/ Z 85.05 21.53%

27 69 57 87 I " r ' " 111" I" " 111111"111 H 11111111" " i" " i1"' i11" i " " i " " 11" 1111" r 11111" 11" " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- —............................. 43 10.20 10.40 10.60 10.80 m/ Z 57.05 15.95% 57 5000 71 85

m/z-> I' ‘ " I ’ " ' I " " I 20 25 30 35 40 l 45 ' I'''' I 50 55 60 M 65 70 TT’T’T 75 80 WTTTT 100 85 90 95 100 105 10.20 10.40 10.60 10.80

26625.D NP112701.M Fri Dec 07 14:48:51 2001 Page 11

NYC-WTC_000031937

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NYC-WTC_000031937Source: NYC Law Department, mirrored locally

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