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GCMS analysis results for sample AD26680, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032058–000032078

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ****************************************************** ** ** ****** * * * * * Peak Number 12 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.51 0.63 ng/uL 169676 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 36 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 25 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 23 4 Hexane, 3-ethyl- 114 C8H18 000619-99-8 17 Abundance Scan 618 (10.512 min): 26680.D (-) m/z 43.05 100.00% 4b

5000

H+ 39 53+4 TT TTTTTmgi 57 61 69 'll.......... ........... 85 V . ' 1 I 10.20 10.40 m/ z 1 TTUPTT 10.60 10.80 65.63% miz-> I " “ I'•' 'I T’T’ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 45.10 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

5000 57 71 85 —AA—A 10.20 10.40 10.60 10.80 m/z 41.10 31.41% 1 100 . I.. 1.... 1.... 1. TTTTTTTT I'1'' I'1 rrp-r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-mnethyl- 45

10.20 10.40 10.60 10.80 5000- m/z .85.05 24.90%

27 69 57 87 i : ■ i'' ■' r ' ■ I • •'111" ’ I 111" I I•“'I 'm/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63547: 2-Pentanol, 4-methyl- TICEECETT p-m । . . . . | 45 10.20 10.40 10.60 10.80 m/z .57.10 17.59% 5000

27 69

miz-> I" “ I 111111 38—444 57 1 87 111 " THHr ' ■' i " ' b " " i''" I'" 11'1" i" ■' i " " r " ' i ■' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 - sA= 10.20 10.40 10.60 10.80

26680.D NP112701.M Fri Dec 07 13:11:48 2001 Page 12

NYC-WTC_000032076

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