GCMS analysis results for sample AD26682, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0501\26682.D Vial: 2 Acq On 5 Dec 2001 9:41 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

10.50 1.06 ng/uL 366386 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 entative ID MW MolForm CAS# Qual

1 Oxirane, /-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 45 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 32 3 Hexane, 2,3,5-trimethyl- 128 C9H20 001069-53-0 27 4 Hydroxylamine, O-hexyl-_____________ 117 C6H15NO 004665-68-3 25 'Abundance Scan 617 (10.502 min): 26682.D (-) m/z 43.05 100.00% 43

5000

57 85 1 1 i • ' 1 ■ ।

150116..... L ■ ' i ■ ■ 10.20 10.40 10.60 10.80 100 • ' ' ' I ' ' ' ' I ' ' 1 1 I 1 111 I I ' I 1 ' 1 1 I ' ' 1 ' I 1 ' ' ' I 1 m/z 45.10 53.57% miz-> 20 30 40 50I 60 70____ 80 90 100 110 120 130 Abundance #1531: Oxirane. 2-methyl-3-propyl-, cis- 43

57 5000 71 85 1 TPP ■ i ■ 1 10.20 10.40 10.60 10.80 m/ z 41.10 27.37% 1 । II ‘ ' i ■ 1 ■ ■ I >i 1....... 11 I ' 1 'I'' ' 1 I 1 100 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1773: 2-Pentanol, 4-methyl- i 45 r-Pr TITTrr , f 10.20 10.40 10.60 10.80 5000 m/ z 85 • 05 21.93%

27 69 57 i > । ■ । ■ i ■ I 87 • i ■ ■ ■ • i • ■ ■ ■ i ■ ■ ■ ■ । ■ 1 ■ • ■ ■ । TTI । । m/z-> Abundance 20 30 40 50 60 70 80 90 100 #65140: Hexane, 2,3,5-trimethyl- 110 120 130 V ■ ■ । ■ ■ ■ ■ । 43 10.20 10.40 10.60 10.80 m/z 57.05 17.10% 5000- 85

U_ 57 27 71

miz-> ... ...... - 20 30 40 50 60 1 70 ‘11 80 90 100 110 ....128 120 130 -A-4 10.20 10.40 10.60 10.80

26682.D NP112701.M Fri Dec 07 13:13:32 2001 Page 11

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