GCMS analysis results for sample AD26679, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26679. D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 12 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

10.51 0.72 ng/uL 247655 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 53 2 2-Hexanol / 102 C6H140 000626-93-7 38 3 2-Hexanol,/3-methyl- 116 C7H160 002313-65-7 38 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 37 Abundance Scan 618 (10,507 min): 26679.D (-) m/z 43.05 100.00% 4b

5000 85 57 • 1 I ' KPPTT i m/z-> Abundance 111111 m +53+mm. . 39

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ■। । 69 100 । ■■■■।■••■।••■■। 10.20 m/z 10.40 10.60 45.10 10.80 65.59% #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 57 -A-A- 5000 71 85 10.20 10.40 10.60 10.80 m/z 41.10 29.11% I 100 I1 ‘ III • " • I •" t («I i•• ■ • i TTTTIT i •• •• i "‘T '....... 11" TUTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol 45 +92 10.20 U_ 10.40 10.60 10.80 5000 m/z 85.0 5 23.88% 1 69 27 31 39 55 1 87 > u I] I ... | . . . . | • i" " r r " ' i " '' r • " i' " • r " ।.... ।...i|11ii1111 > । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3372: 2-Hexanol, 3-methyl- ■ ■ i ■ • • ■ i ■ I 1 1 ■ ■ i 1 ' ■ ' i I 415 10.20 10.40 10.60 10.80 m/z 57.10 17.84% 5000

27 70

m/z-> 4 56 , 83 98 " I''" i.......... "1 1" ' i" " r '1' i'11 • i " " r '111" " I " 111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 - -A- p 10.20 10.40 10.60 10.80

26679.D NP112701.M Fri Dec 07 13:10:23 2001 Page 12

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