GCMS analysis sample AD26537, non-target compounds, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\l\DATA\DEC0701\26537.D Vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 10.52 1.93 ng/uL 515831 1,4-Dichlorobenzene-d4 11.88 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 36 2 2-Hexanol 102 C6H140 000626-93-7 35 3 2-Pentano , 4-methyl- 102 C6H140 000108-11-2 32 4 2-Hexanone, 3,3-dimethyl-___________ 128 C8H160 026118-38-7 25 Abundance Scan 619 (10.519 min): 26537.0 (-) m/z 100.00% 43

5000

57 85 ‘ ‘ i • T 39 Til. 53,,||. ii69 , . 100 10.20 10.40 10.60 10.80 T1090111292——01—Tpummf —ngnd,—m—p—pmmp—uamuoogonaf 11» j j’l 11 rj 111 i 11 i'i) 11 j 111 m/z m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 57 5000 71 85 ’II 10.20 10.40 10,60 10.80 m/z 41.05 26.97% 100 1’11111021111—0111117317 '11'!" " i T' rI 1111 n I ■n-p-n-rp-rT “' ‘ I' “ ‘ 111 “ 11" 11' “11 mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol 45 Per — -।------- 10.20 10.40 10.60 10.80

1A_ 5000 m/z 85.15 20.27%

69 27 31 39 55 87 t i । i : » ij i l i « j I i i « । « : i i । i l t I 1 I i i ] i i i i | i i I i | i < : j । i n j । 1i । : t : i | » j i i | i i i i | I j 1 i j i j । i i: i ] 1 1 I I| miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1773: 2-Pentanol, 4-methyl- 45 10.20 10.40 10.60 10.80 m/ z 57.10 15.99% 5000

m/z—> 27 .i 57 T 87 > p > > . p l > . p . • > p > I > p I l l | I > . > p . . > | I I 1 I | I I I I | I ] I | | l ) I | p ■ . . p | I l p I . | | 1 1 | ■ | V. I I | I I I 1 | I I I I |

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 U_ 10.20 10.40 10.60 10.80

26537.D NP112701.M Thu Dec 13 11:27:34 2001 Page 13

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