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GCMS calibration table for TCLP analysis, Dec 5 2001

Machine-extracted title · confidence 100%

Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.

NYC-WTC_000032142–000032159

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 8 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

10.50 0.81 ng/uL 283922 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2 /methyl-3-propyl-, cis- 100 C6H120 006124-90-9 38 2 2-Pentanol , 4-methyl- 102 C6H14O 000108-11-2 38 3 2-HexanoT 102 C6H140 000626-93-7 35 .4 2,5-Hexanediol 118 C6H14O2 002935-44-6 33 Abundance Scan 617 (10.503 min): 26712.D (-) m/z 43.10 100.00% | 43

miz-> 5000-

20 25 30 35 39 — ‘ 1‘ 61 5344 - - 57 69

40 45 50 55 60 65 70 75 80 85 TH 85

I>.I>lI.iqnlil 90 95 100 105 10.20 10.4G 10.60 10.80 m/z J LN 45.10 —PP 59.51% Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

5000- 57 71 85 -AAP 10.20 10.40 10.60 10.80 m/ z 41.10 27.50% I! 100 i I •"' I * > I • 11'111 TT’TT I"'‘l*’“I‘ '’I miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance i 45 #1773: 2-Pentanol, 4-methyl-

— $— ■ I T 1 10.20 10.40 A 10.60 11*‘T 10.80 5000 m/z 85.05 20.43%

27 69 i 57 87 " i " " i ‘ . .............................. mpe i " ■' i" ■ ‘ r •" i r "111111111111' TTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1792: 2-Hexanol ' U ' ' ° l ' i ■ ■ ' ' i ■ ' ■ ■ I 45 10.20 10.40 10.60 10.80 m/z .57.10 15.31% 5000 -

m/z- ‘IIT+473031..35 3940.4445 50 5555 60 65 6970 75 80 8587 90 95 100 105 20 25 TT TPTT pu I I | I I I I | I • I I | I I I I | ill . | I I TTTT I I UA _ - TEIErIT i i r. 10.20 10.40 10.60 10.80

26712 .D NP112701.M Fri Dec 07 13:15:21 2001 Page 8

NYC-WTC_000032155

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NYC-WTC_000032155Source: NYC Law Department, mirrored locally

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