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GCMS Analysis Report for Sample AD26386, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26386 with a note regarding unknown compounds.

NYC-WTC_000031415–000031432

Folder label: “GCMS X 11/5/01 A 12/1/01

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Scanned page image, NYC-WTC_000031430
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26386.D Vial: 12 Acq On : 30 NOV 2001 10:13 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 10.53 0.86 ng/uL 384399 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 23 3 Hexane, 2 ,3, 5 - trimethyl - 128 C9H20 001069-53-0 16 4 Pentanal,2,2-dimethyl- 114 C7H140 014250-88-5 16

(i Abundance • Scan 621 (10.533 min): 26386.D (-) m/z 100.00% 43

5000

57 85 TTT 10.20 10.40 10.60 10.80

miz-> 20 ‘ I ‘ ’ i ' 30 —451 40 . .... 50 60 70 80 . 90 100 100 TT J I : 18 i TT * j * 1 1 1 1 * * * * 1 ) T 110 120 130 m/z 45.10 41.21% Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

57 5000 71 85 10.20 10.40 10.60 10.80 m/z 41.10 29.00% 100 miz—> — 20 ....30—....40Ill -l-r-p-r 50 ' i ■ • ■ ■ i1 60 70 80 —————————————— 90 100 110 120 130 Abundance #8516: Hexane, 1-propoxy- 43

10.20 10.40 10.60 10.80‛T 5000 m/z 85.05 23.94% 56 85 73

miz-> Abundance •............ 1 11— I 11। 1 1‘ 20 30 40

43 50 60 70 80 4 4 90 100 110 120 130 #5161: Hexane, 2,3,5-trimethyl- 1 . 10.20 10.40 10.60 10.80 m/z 57.10 19.42% 5000 85

A 57 71 27 . I ■ ■ ■'. I...... TT—UTT 1 1l. 11 i 1 ‘ 1 • I 1 ■ ■ ■ i ■ tr I ‘ 128 * J ‘ 11 » j ‘ ‘ * 1 1 1 * ‘ ‘ 1 * 1 TTTr ■ 11E1T T’rrT mfz-> 20 30 40 50 60 70 80 90 100 110 120 130 10.20 10.40 10.60 10.80

26386. D NP112701.M Tue Dec 04 10:38:37 2001 Page 8

NYC-WTC_000031430

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NYC-WTC_000031430Source: NYC Law Department, mirrored locally

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