GCMS analysis report for sample AD26393, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26393.D Vial: 3 Acq On : 30 Nov 2001 2:02 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 10.53 0.84 ng/uL 362022 l,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 Hexane, 2-methyl- 100 C7H16 000591-76-4 27 3 Hydroxylamine, 0 - hexyl - 117 C6H15NO 004665-68-3 25 4 Hexane, jf, 3,5-trimethyl-____________ 128 C9H20 001069-53-0 25 Abundance Scan 620 (10,529 min): 26393.D (-) m/z 43.10 100.00% 43

5000

- +4 151 11— — j-i । i — 57 100 1 ■ ।1 * * * । * ■ 69 85 JU. TT 1 TTur 1 10.20 10.40 10.60 10.80 m/z 45.10 40.99% m/z-> 20 30 40 50 60 70 80 90 ___________________________________ 100 110 120 . . ............ Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 57 5000 71 85 TIT 10.20 10.40 10.60 10.80 m/z 41.05 26.35%

miz-> 20 —... J 30 40 t-r-r-r 50 —P 80 90 100 110 100 120 Abundance

5000 43 #63433: Hexane, 2-methyl-

frTT JU 1Iff 10.20 10.40 10.60 10.80 m/z 85.05 21.68% 57 85 27 , . ,1 . , , ,1 1 13m I 11 71 ' i ■ ■ ■ ■ i ■ ' • i ■ 1 1 •' 100 I 1 ' • ‘ I ■ • • • I ‘ ‘ ■ I • ‘ miz-> 20 30 40 50 60 70 80 !90 100 110 120 Abundance #3421: Hydroxylamine, O-hexyl- TTpuupurmrLg)—T 43 10.20 10.40 10.60 10.80 m/z57.10 18.01%

5000

56

m/z—> TLTIIuTT 20 30 — L 40 50 69 .79 I 85 91 ■ I 1 ' 1 1 I r 1 1 1 I1 1 1 • । • • • • i ■ • » ■ । • ■ • ■ । 60 70 80 90 100 110 117 120 ■ —A . 10.20 10.40 10.60 10.80

26393.D NP112701.M Tue Dec 04 10:43:51 2001 Page 8

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