GCMS Analysis Report for Sample AD26336, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3 001\26336.D Vial: 30 Acq On : 1 Dec 2001 2:36 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.78 ng/uL 250827 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2,2-ydimethyl-3-propyl- 114 C7H140 017612-35-0 20 2 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 17 3 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 17 42,2-Dimethyl-1,3-propanediamine 102 C5H14N2 007328-91-8 12 Abundance Scan 598 (10.323 min): 26336.D (-) m/z 43.10 100.00% 43

5000 59

73 85 —==PPrre --- i| iTi i i j

miz-> -3, + top 53 Tm 10131 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 120 100 “'11 ‘‘ I ‘ ‘ ‘ ‘ I “ ‘ ‘ I'‘ I ‘ ‘ ‘ ‘ I' ‘‘ I “ ‘ 10.00 10.20 10.40 10.60 m/z 59.10 40.58% Abundance #3003: Oxirane, 2,2-dimethyi-3-propyl- 43 50 85

5000 IPPPTTAIT 10.00 10.20 10.40 10.60 72 m/z 55.10 35.47%

miz—> 4 -9 30 35 40 45 50 55 60 €5 70 75 80 85 90 95 100 105110115120' Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 -A 10.00 10.20 10,40 10.60 ' 57 5000 71 85 m/z 41.10 34.50%

mtz-> ..... l ■ i"1 ■ i ■ ”11 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 120 100 Illi I I III [TCgnr

Abundance 43 #8516: Hexane, 1-propoxy- 444 । • 10.00 10.20 10.40 10.60 MA— m/z 57.10 34.49% 5000

m/z—> 56 61 73 Y K mmmmm rpmm-mmmm 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115120 ■ ■ i ■ • L . I ‘ ‘ ‘ 1 I * * ' ' I 10.00 10.20 10.40 10.60

26336.D NP112701.M Tue Dec 04 15:07:52 2001 Page 6

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