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GCMS analysis report for sample AD26472, Dec 2001

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DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26472 noting other unknown compounds.

NYC-WTC_000031611–000031623

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26471.D Vial: 11 Acq On 30 Nov 2001 9:19 pm Operator: GALOS Sample 2 gc/ms unknown 11/3 Inst GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.33 0.42 ng/uL 193033 1,4-Dichlorobenzene-d4 11.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2,2 dimethyl -3-propyl- 114 C7H140 017612-35-0 28 2 Oxirane, 2/methyl-3-propyl-, cis- 100 C6H120 006124-90-9 23 3 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 23 4 Oxirane, 2-butyl-3-methyl-, cis- 114 C7H140 056052-93-8 23 Abundance " Scan 598 (10.328 min): 26471.D (-) m/z 43.10 100.00% 43

5000 57 73 85 A10.00 10.20 10.40 10.60

m/z—> mll 4+5341 — 100 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115120 I I I 11I 11 I|I I 11111 I 11I 11 1|TTI 111111|111 m/z 57.10 34.04% Abundance #3003: Oxirane, 2,2-dimethyl-3-propyl- 43 59 85

5000 - 4 44. । 10.00 10.20 10.40 10.60 72 m/z 55.10 33.38%

m/z—> 1’111117111 Imp Ip ..JU.... 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115120 1 . ..............99 I............ ... i.i.p.i.p..ip...piiipiiipiiipn ............... .

Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 .10.00 — ....10.20 A— 10.40 10.60 57 5000 71 85 m/z 59.10 31.19%

m/z—> mlll Tupana 100 •I" "I1 “11 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 115 120 1........ ।.... 11 ...r. 1111111111111111

Abundance #8516: Hexane, 1-propoxy- 43 10.00 10.20 10'40 10.60 ' m/z41.10 29.95%

5000

56 85 73

m/z—> m m 11 61 — 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 120 |. >4 >]>>.. pill | T 1444 A A WM4 10.00 10.20 10.40 10.60

26471.D NP112701.M Tue Dec 04 10:44:26 2001 Page 3

NYC-WTC_000031621

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NYC-WTC_000031621Source: NYC Law Department, mirrored locally

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