GCMS calibration table for method 208, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26252.D vial: 18 Acq On : 1 Dec 2001 3:40 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxirane, 2,2-dimethyl-3-propyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.41 ng/uL 192754 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2,2-dimethyl-3-propyl- 114 C7H140 017612-35-0 32 2 Hexane, 2-metbyl- 100 C7H16 000591-76-4 22 3 Oxirane, 2-m0hyl-3-propyl-, cis- 100 C6H120 006124-90-9 12 4 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 12 Abundance Scan 598 (10.322 min): 26252.D(-) m/z 43.10 100.00% 43

5000 59

73 85 1.11 mPrr n 10.00 10.20 10.40 10.60

miz-> 20 — —- 30 40 +53+ I l 50 60 70 80 100 ' i 1 ‘ 1 1 1 1 1 1 1 1 ‘ 90 100 । । 1 • 1 1 1 1 110 120 m/z 59.10 | 39.39% Abundance #3003: Oxirane, 2,2-dimethyl-3-propyl- 43 59 85

--------------------- 5000 10.00 10.20 10.40 10.60 72 m/z 55.10 34.21% 99 I 114 1 i ‘ • i ■ ■ ■ ■ i ■ • ■ • i • miz-> 20 30 40 50 60 70 90 100 110 120 Abundance #63434: Hexane, 2-methyl- 43 -----A 10.00 10.20 10.40 10.60 5000 m/z 57.10 33.57% 57 85 29 69 , 100

LM_ __ I I ■ 'i1 n—Tir ■ i ■ ' ' ' i ' ‘ 1 ' i 1> I i > | r . . . | . i । i i i i । i mlz-> 20 30 40 50 60 70 80। 90 100 110 120 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- AMAm — 4 10.00 10.20 10.40 10.60 m/z41.10 29.22% 57 5000 71 85

- 100 ■ > I •• 1 I .... J ... 1 I J IA A/ 1— 1 i 1 ■ ■ 1 I 1 1 * I 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 10.00 10.20 10.40 10.60

26252.D NP112701.M Tue Dec 04 10:11:06 2001 Page 3 N YC- WTC_000031233