GCMS calibration table for method 208, Nov 2001

Machine-extracted title · confidence 90%

Calibration data table listing response factors for polycyclic aromatic hydrocarbons and other compounds.

NYC-WTC_000031223–000031235

Folder label: “GCMS X 11/3/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26252.D vial: 18 Acq On : 1 Dec 2001 3:40 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.50 ng/uL 239880 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 95 2 Benzene-1,2/3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzofuran/ 7-chloro- 152 C8H5C1O 024410-55-7 9 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 9 Abundance Scan 754 (11.752 min): 26252.D (-) m/z 150.00 100.00% 150

5000 115 78 — — -

40 . . 63 - — Wpgr 52 87 11,40 11.60 11.80 12.00 m/z 152.00 66.11% 1111 mm miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

115 ...................... — ...... । , irr( r . . .................. । . . . .। . 5000 78 11.40 11.60 11.80 12.00 52 m/z 115.05 42.25% 35 87 1 T-L—n-tuur ‘111 • '' 111 12Wmamg 1111 ■1 • i1 ■111 • ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 /.............. —i । । . i . < । i . r r । . . . n । i i । i । j 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 24.37%

35 87 ........................ , T’I ■ ■' I '' ‘ ■ i ' ■ 111'11'' +1'1 »• l < ■ ■ > l ■ ■ miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ■ — — Abundance #10136: Benzofuran, 7-chloro- 212/1/1/1 P TIT T 152 11.40 11.60 11.80 12.00 m/z 52.10 19.85% 5000 89

63 49 .11 73 35 —Hpmtee ' i' ■ ■ 11' ‘ ‘ ■ i ‘125 । . ; . . i । । ... i ] , i > i, r. i i । i ■ 1 * 11 ‘ ‘ ' i ■ 1 ■ ■ i ‘I[1 • 1 i 1 • ‘ ■ i • - m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26252.D NP112701.M Tue Dec 04 10:11:06 2001 Page 4 NYC-WTC_000031234

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