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GCMS Analysis Report for Sample AD26387, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26387 with a note regarding unknown compounds.

NYC-WTC_000031433–000031451

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26387.D vial: 13 Acq On : 30 NOV 2001 11:08 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 l,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.53 ng/uL 256985 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 1, 4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 59 2 Benzene — ,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 45 3 Benzal ehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 Biphe: lene 152 C12H8 000259-79-0 9 Abundance Scan 754 (11.752 min): 26387.D (-) m/z 150.00 100.00% 150

5000- 115 78 - 52 11.40 11.60 11.80 12.00 -H 40 — I 1 T’87 T i i ■ i | ■ i i | TTTI । i । । i , i i i 1 | i > | I— m/z 152.00 62.24% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

.............................. ............... 5000 115 78 11.40 11.60 11.80 12.00 52 m/z 115.05 36.79% 35 87 1 ■ i ■ ■ ■ ‘ I ‘• i 1’1/161111 i ■ ■ ■ • i ■ ■111 ‘ ‘' i < i • •»• i < • • • । • mlz-> 30 40 50 60 70 80 90 110 120 130 140 150 160 100 Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro- 150 —T I I I II I I T / [ ♦ ♦ • • 1 • • * • I •

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 ’ 24.00%

35 87 — ■11 ■ ■ ■11 ■ ■ —I ■ I " " I'1 1— miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.40 11.60 11.80 12.00 ' m/z 52.00 . 19.48% 106 5000- 53 81

122

m/z—> 1’11411 m-r-p 30 40 50 - 60 70 92 — ■ i1 ■ |... 4136.... 11 1 ■ I ■ 80 90 100 110 120 130 140 150 160 - — /............... 11.40 11.60 11.80 12.00

26387.D NP112701.M Tue Dec 04 10:39:17 2001 Page 10

NYC-WTC_000031450

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NYC-WTC_000031450Source: NYC Law Department, mirrored locally

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