GCMS Analysis Report for Sample AD26390, Dec 2001

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Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.

NYC-WTC_000031491–000031508

Folder label: “GCMS X 11/5/01 A 12/1/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D vial: 4 Acq On : 30 Nov 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 1,4-Dichlorobenzene-d4 Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.50 ng/uL 217734 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance Scan 753 (11.747 min): 26390.D (-) m/z 150.00 100.00% 150

5000 115 78 52 mT 11.40 11.60 11.80 12.00 ■ > । > । ’ r11 ।.,1.......... • ■ i......... TP +444 r ' 87 40 HH —30 11 ■ । < > 111’113 1 m/z 152.00 59.96% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150 ..................................................

5000 115 78 11.40 11.60 11.80 12.00 52 m/z 115.05 38.56% 35 87 - ■ • i • • ■ ■ i * ■ • ■ i 1’2’2115 IPBng I । i i । । । • > > 11 . > mlz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 —......... — 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 25.86%

35 87 — 1 111 — 1 11I""I'1 — T —TIBIPPg miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 152 11.40 11.60 11.80 12.00 m/z52.00 21.28% 106 5000 53 81

122 1 ‘ i1 • • ‘ I • ■ ■ • i1 ■ ■ i ‘ 1 •' 1'1 ‘Ir 92 — I TTT136 1 : : j J • * I j TTsr - ' * I ' ■ ' ' I ' m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26390.D NP112701.M Tue Dec 04 10:41:46 2001 Page 9

NYC-WTC_000031507

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GCMS analysis report for sample AD26392, Dec 2001 · Box DEP Box 21

NYC-WTC_000031530

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26392 noting other unknown compounds.

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