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GCMS Analysis Report for Sample AD26390, Dec 2001

Machine-extracted title · confidence 100%

Laboratory comment confirming detection of Butylbenzylphthalate in sample AD26390 on December 10, 2001.

NYC-WTC_000031491–000031508

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26390.D vial: 4 Acq On : 30 Nov 2001 2:57 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library 1 C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 10.54 0.58 ng/uL 249836 1,4-Dichlorobenzene-d4 11.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 36 2 Pentane, 2,4-dimethyl- 100 C7H16 000108-08-7 27 3 Pentanal, 2,2 - dimethyl - 114 C7H140 014250-88-5 25 4 Hexane2,3, 5-trimethyl- 128 C9H20 001069-53-0 25 Abundance Scan 621 (10.536 min): 26390.D (-) m/z 43.10 100.00% 43

5000

57 85 ------A 69 10.20 10.40 10.60 10.80 100 —u—11—01—01—0060"10711T TpH H m/z45.10 46.38% m/z—> 5 10 15 20 25 3035404550556065 70 75 80859095 100105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43

5000 57 71 85 TIr AAL 10.20 10.40 10.60 10.80 m/z 41.05 27.75%

miz—> .kk.[.> ji। lll fm 100 Duppnur —p 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63424: Pentane, 2,4-dimethyl- 43 57 PPP ■ 10.20 10.40 10.60 10.80 5000 m/z 85.05 23.14% 27 85

_A.... 15 69 mmmpm fumm *pp—p—mp—n—p—mnm "———10 100 —011133111 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #3038: Pentanal, 2,2-dimethyl- 43 10.20 10,40 10.60 10.80 ‘ m/z 57.10 18.17% 5000 85 27 57

m/z—> 1mp 4 TTTTT TTp-rrq 5 10 15 20253035404550556065 70 75 80859095 100105 —A - 10.20 10.40 10.60 10.80

26390.D NP112701.M Tue Dec 04 10:41:46 2001 Page 8

NYC-WTC_000031506

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