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GCMS Analysis Report for Sample AD26336, Dec 2001

Machine-extracted title · confidence 100%

Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.

NYC-WTC_000031384–000031399

Folder label: “GCMS X 11/5/01 A 12/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26336.D Vial: 30 Acq On : 1 Dec 2001 2:36 pm Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 10.53 0.66 ng/uL 211080 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 38 2 2-Hexanol,/3-methyl- 116 C7H160 002313-65-7 35 3 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 32 4 2-Hexanol 102 C6H140 000626-93-7 25 Abundance Scan 621 (10,534 min): 26336.D (-) m/z 43.05 100.00% 4

5000

39 57 69 85 A TrTrr i i (TT i i । i i 10.20 10.40 10.60 10.80

miz-> mmmm m —5 -dmmm WpgT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 45.00 62.77% Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 43 57 5000 71 85 T i 1 0 i 1 ' 1 ' r 1— 10.20 10.40 10.60 10.80 m/z41.10 31.49%

»— _ 1 100 mm + Opuu ■ ।' ■ ■ • i ■ ■ ■' । H miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3372:2-Hexanol, 3-methyl- 45 A 10,20 10,40 10,60 10,80 5000 m/z 85.05 22.13% 70 56 83 98 WU mH 111.11. i. । >... । TWTNI i'11 ■ i mlz-> 2025303540 45 50556065 70 75 80859095 100 105 Abundance #1773: 2-Pentanol, 4-methyl- 45 10.20 10.40 10.60 10.80 m/z 57.10 17.40% 5000

69

m/z—> m 27 trpHp 57

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 i 87 • 4 i ■ • __ 10.20 10,40 10.60 10.80

26336.D NP112701.M Tue Dec 04 15:07:53 2001 Page 7

NYC-WTC_000031398

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NYC-WTC_000031398Source: NYC Law Department, mirrored locally

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