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GCMS comments for sample AD26476 showing no non-target compounds

Machine-extracted title · confidence 100%

Analysis report dated December 16, 2001, stating that mass spectrometry of sample AD26476 revealed no non-target compounds.

NYC-WTC_000031707–000031728

Folder label: “GCMS X 11/6/01 A 12/7/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0701\26476.D Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Oxirane, 2-methyl-3-propyl-, c Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

10.52 1.88 ng/uL 673359 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentati ID MW MolForm CAS# Qual

1 Oxirane, 2-methyl-3-propyl- , cis- 100 C6H120 006124-90-9 45 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 38 3 2-Hexanol / 102 C6H140 000626-93-7 35 4 2,5-Hexanediol ____________ _______ 118 C6H14O2 002935-44-6 28 Abundance ’ Scan 619 (10.516 min): 26476.D (-) m/z 43.05 100.00% 4b

5000 85 J I ’• ' 'I 1 ' TTT ‘ T I 39 57 61 69 10.20 10.40 10.60 10.80 11 r — 1 •t-rrryr 53+4—.... H +* 100 m/z 45.10 62.08% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-, cis- 4 57 5000 71 85 '■ri T T TT 10.20 10.40 10.60 10.80 m/ Z 41.05 29.55%

m/z-> 3 •' I ’ " ' I 100 11'11 ’ I ” '' I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ।। ' i ■''' ।।

Abundance #1773: 2-Pentanol, 4-methyl- 45 P — —PP 10.20 10.40 10.60 10.80 5000 m/z 85.05 21.82%

27 69 57 i 87 I i! '1 r1 I’’" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63583: 2-Hexanol -' ' i''' - I 45 10.20 10.40 10.60 10.80 m/z 57.05 16.72% 5000-

J A 69 55

m/z-> ‘IIT 47,31,39.4 TPH ' r''' i " ‘' r 1VPguTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 87 1 ■r-f-r-r TII 10.20 10.40 10.60 10.80 i 1 1 ' 'I

26476.D NP112701.M Thu Dec 13 11:21:05 2001 Page 13

NYC-WTC_000031727

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NYC-WTC_000031727Source: NYC Law Department, mirrored locally

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