GCMS comments for sample AD26476 showing no non-target compounds

NYC 9/11 Public Portal Document Library Search Compound Report

Data File c:\HPCHEM\1\DATA\DEC0 701\26476.D Vial: 6 Acq On 7 Dec 2001 10:40 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexane, 1-propoxy-■ Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.30 3.47 ng/uL 1243260 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 1 -prop Y- 144 C9H20O 053685-78-2 25 2 Oxirane, 2 -mi,thyl-3-propyl-, cis- 100 C6H120 006124-90-9 23 3 Pentane, 2 3,3-trimethyl- 114 C8H18 000560-21-4 23 4 Oxirane, -butyl-3-methyl-, cis- 114 C7H140 056052-93-8 17 Abundance Scan 596 (10.305 min): 26476.D (-) m/ z 43.10 100.00% 43

5000 55 59 / 85 73

m/z-> I" '' I' " ’ I l 39 51 . ............ .. t .....I............ TTTTTITT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 p-rr 89 100 10.00 10.20 10.40 m/ z 59.10 10.60 32.12% Abundance #8516: Hexane, 1-propoxy- 43

5000 10.00 10.20 10.40 10.60 56 85 m/ z 55.10 30.72% 73 ■ ■ ।' r "' i — 39 m 61 11" 11 69 ■>। | >11 PH 111 ’ * I I" ” I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1531: Oxirane, 2-methyl-3-propyl-. cis- 43 TIT — — 10.00 10.20 10.40 10.60 57 5000 71 85 m/ z 57 • 10 30.72% i

"i""i i • r 1 " 11'111 • i ■ ■ ■' I ■ l‘“•I 100 TTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #3088: Pentane, 2,3,3-trimethyl- , J 11.1 43 10.00 10.20 10.40 10.60 m/ z 41.10 29.36% 5000 71 57 85 27

m/z-> X TH ............. f 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 99 । ■ । ■ > । > <111 i" " i TTCT ■p .trt 10.00 10.20 10.40 10.60

26476.D NP112701.M Thu Dec 13 .11:21:03 2001 Page 12

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