GCMS analysis report for sample AD26434, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26434.D Vial: 22 Acq On : 1 Dec 2001 7:18 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Misc. 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Hexane, 1-propoxy- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.32 0.42 ng/uL 200708 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 23 2 Oxirane, 2-metnyl-3-propyl-, cis- 100 C6H120 006124-90-9 17 3 Ether, 3-butenyl propyl 114 C7H140 034061-75-1 17 4 Oxirane, 2butyl -3 -methyl -, cis- 114 C7H140 056052-93-8 17 Abundance ’ Scan 597 (10.319 min): 26434.D (-) m/z 43.10 100.00% 43

5000

20 55 59 73 85 AUU r TTITT111T I ‘Ith . . I I I 10.00 10.20 10.40 10.60 T

11P1111 ’l 11111 “ 11 “ I +++ ---mHmmmm 1 1 51 1 89 ... 11।|( 100 m/z 59.1036.73% m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #8516: Hexane, 1-propoxy- 43

5000 1 » i * * ■ ■ i > * ‘ ‘ I 10.00 10.20 10.40 10.60 56 85 m/z 55.10 35.47% 61 73 =====*=*== - mk mz-> 20 25 30 35 40 #1531: Abundance 45 50 55 60 65 70 75 80 85 90 95 100 105 Oxirane, 2-methyl-3-propyl-, cis- 43 11 I1 1 1 1 I1 '' WA 10.00 10.20 10.40 10.60 57 5000 71 85 m/z 57.10 30.31%

100 *MH 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 1 miz-> Abundance 40 #3059: Ether, 3-butenyl propyl Amer 10.00 10.20 10.40 10.60 m/z 41.10 29.41%

5000

55 73 85 30 1' m nt IHm 11 111 H 1111 |ii 1111.1.1 |. I|J| , A A-AA-AAPPmA/ n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.00 10.20 10.40 10.60

26434.D NP112701.M Tue Dec 04 15:41:40 2001 Page 3

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