GCMS analysis report for sample AD26434, Dec 2001

Machine-extracted title · confidence 100%

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26434 noting other unknown compounds.

NYC-WTC_000031592–000031601

Folder label: “GCMS X 11/5/01 A 12/1/01”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26434.D Vial: 22 Acq On 1 Dec 2001 7:18 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins MiSG : Multiplrs 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 l,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.74 0.51 ng/uL 244388 1,4-Dichlorobenzene-d4 11.89 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 4-Amino-2 chlorobenzonitrile 152 C7H5C1N21 ____ 020925-27-3 10 Abundance Scan 752 (11.740 min): 26434.D (-) m/z 150.00 100.00% 150

5000 115 52 78 -A 11.40 11.60 11.80 12.00 40 .. ....... 1... .... I ‘ 1- miz-> -H3 ■ * i1 30 40 50 60 I * ‘‘ I 1’211111117 • ‘ ‘ 1’1111’111177 80 90 100 110 120 130 140 150 160 m/z 152.00 . 67.47% Abundance #9593: 1,4-Dichlorobenzene-d4 150

5000 115 T IUTIr TT । 4 $ । — । । r 78 11.40 11.60 11.80 12.00 52 m/z 115.05 43.13% 35 ■ • i ■ ■ ■ ■ i'''' i ' ' I ■''11 ■ ■ 87 .1 i11 ■11111111111 TT TTIm—tnr I miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 ------------------- 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 25.12%

35 87 I_______ ' i •111111111 i ■'' ■ i ■ ' ' ■ i 11 ■ ■ i ■ ' ■' i' 1 I—— miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- • > — - 152 11.40 11.60 11.80 12.00 m/z 52.00 22.99% 106 5000 53 81

- 122 • ■ i ‘ • • ■ i ■ ■ •' i ’4111 ’111 92 TITITT 136 1' I ' ----- miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

26434.D NP112701.M Tue Dec 04 15:41:40 2001 Page 4

NYC-WTC_000031600

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000031600Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis report for sample AD26474, Dec 2001 · Box DEP Box 21

NYC-WTC_000031650

DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26474 noting other unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998