Laboratory report documenting GCMS analysis of sample AD26320 with unidentified compounds detected.
NYC-WTC_000031319–000031332Folder label: “GCMS X 11/3/01 A 12/1/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library search Compound Report Data File C:\HPCHEM\1\DATA\NOV3001\26320.D vial: 19 Acq On 1 Dec 2001 4:35 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins M1SC : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.75 0.53 ng/uL 296425 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 96 2 Benzene-1,/, 3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 53 3 Benzalde: yde, 2-hydroxy-3-methoxy- 152 C8H803 000148-53-8 35 4 Benzoic j cid, 2,5-dimethyl- 150 C9H10O2 000610-72-0 9 Abundance Scan 753 (11.749 min): 26320.D (-) m/z 150.00 100.00% 150
5000 115
—+ 52 78 — —— 40 11.40 11.60 11.80 12.00
miz-> — ■ ■ । ■ 3b ++63 I—— m/z 152.00 40 50 60 70 80 90 100 110 120 130 140 150 160 62.86% Abundance #9593:1,4-Dichlorobenzene-d4 150
5000 115 52 78 11.40 11.60 11.80 12.00 " 1 ' m/z 115.05 40.81%
miz-> 35 T TIr n i 11 m-| 30 40 50 11 i1 ■ ■ ■ i ■1 87 i1 ‘ •11 ‘1 ■ ■ i ■1 60 70 80 90 100 110 120 130 140 150 160 TTITTgT I I— Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 150 IIT PPP 11 A PIPP 115 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 23.06%
35 87 - ‘ I ‘' I ' 1 T-p-m-p T I 111 T 111 ' ' I ‘ 1 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- \............... 1' । ■ ■ ■ • । ■r r । TI—T * ‘ i ' 152 11.40 11.60 11.80 12.00 m/z 52.00 21.34% 106 5000 53 81
92 122 , |....... ... ......... 136.......... | 1LLT i 11 1’14’, ■ ’ i1 ■ ■ ‘ i' ■ ‘1‘ —IPPI Tt-t 1‘ ‘1i‘tt771rrTTTTTTTI ■r-rp- miz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 1140 11.60 11.80 1200 ' ' '
26320.D NP112701.M Tue Dec 04 10:13:06 2001 Page 4
NYC-WTC_000031330
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NYC-WTC_000031579
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26433 noting other unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031611
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26472 noting other unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031284
Laboratory report documenting GCMS analysis of sample AD26318 with unidentified compounds detected.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031223
Calibration data table listing response factors for polycyclic aromatic hydrocarbons and other compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031567
DEP lab report dated December 4, 2001, documenting GCMS analysis of sample AD26394 noting other unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031262
Laboratory report documenting GCMS analysis of sample AD26316 with unidentified compounds detected.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031248
Laboratory report documenting GCMS analysis of sample AD26315 with unidentified compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031104
Laboratory report documenting GCMS analysis of sample AD26202 with unidentified compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031384
Report documenting GCMS analysis of sample AD26336 with a note regarding unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031333
Laboratory report documenting GCMS analysis of sample AD26321 with unidentified compounds detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031624
Gas chromatography-mass spectrometry analysis of sample AD26472 identifying unknown compounds, analysis conducted December 4, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000031359
Laboratory comment confirming no non-target compounds were detected in sample AD26203 on December 10, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000031209
Single-page GCMS document identifier from the Environmental Protection Department archive covering late 2001 testing records.
Filed in the same folder
NYC-WTC_000031210
Document header page for GCMS analysis records from the DEP Box 21 collection dated December 2001.
Filed in the same folder
NYC-WTC_000031213
Data table containing pH and volume measurements associated with GCMS method 208 analysis procedures.
Filed in the same folder
NYC-WTC_000031223
Calibration data table listing response factors for polycyclic aromatic hydrocarbons and other compounds.
Filed in the same folder
NYC-WTC_000031236
Laboratory report documenting GCMS analysis of sample AD26252 with unidentified compounds detected.
Filed in the same folder