NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV3001\26318.D vial: 28
Acq On : 1 Dec 2001 12:46 pm Operator: GALOS
Sample : gc/ms unknown 11/3 Inst : GC/MS Ins
Mise 2 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator)
Title : 208 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.75 0.51 ng/uL 243391 1,4-Dichlorobenzene-d4 11.89
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,4-Dichlorobe: ene-d4 150 C6C12D4 003855-82-1 96
2 Benzene-1,2,3 -d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42
3 Benzaldehyde 2 - hydroxy-3 -methoxy- 152 C8H803 000148-53-8 35
4 4-Amino-2-c orobenzonitrile 152 C7H5C1N2 020925-27-3 10
Abundance Scan 753 (11.748 min): 26318.D (-) m/z 150.00 100.00%
150
5000- 115 .................................. ...............
78
52
11.40 11.60 11.80 12.00
miz-> 30
40 87
-HH 63 _ 11TI ——— — 1—— m/z 152.00
111 ‘ 111 ii
40 50 60 70 80 90 100 110 120 130 140 150 160
62.39%
Abundance #9593:1,4-Dichlorobenzene-d4
150
5000 115 T
78 11.40 11.60 11.80 12.00
52 m/z 115.05 39.84%
87
35
• ‘ 1 * 1 ‘ ' I ‘ 1 1 1 1 ■ ■ । * i ■ • -PPP— 'I1' I.... 1.... 1. ■ 1 ——
miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160
Abundance #9592: Benzene-1 ,2,3,4-d4-, 5,6-dichloro-
150
‘ - m ■' TT
115 11.40 11.60 11.80 12.00
5000 52 78 m/z 78.05 25.75%
35 87
mfz->
‘ • i • ■ • * I •1 • ‘ i
30 40 50 60
I ‘ •11 ‘ ‘
70
_.........................
i * • * * i' 4 * > i' * ‘
80 90
i * ’
100 110 120 130 140 150 160
I———
Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- i।jiiii]ii n-1r.. i।....।.
152 11,40 11.60 11.80 1200
m/z52.00 20.66%
106
5000 53
81
122
m/z—>
'' I'''' I ‘'1 I
30 40 50
' u " ' I TT
60 70 80
92
■ । ■ • • • 11 ■ ■ ’[I
90
-13
100 110 120 130 140 150 160
■ ‘ I ‘
-
11,40 11.60 11.80 12.00
26318.D NP112701.M Tue Dec 04 10:12:44 2001 Page 4
NYC-WTC_000031295
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