GCMS analysis results for sample AD26318, Dec 2001

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Library Search Compound Report Data File 2 C:\HPCHEM\1\DATA\NOV3001\26318 .D Vial: 2 8 Acq On : 1 Dec 2001 12:46 pm Operator: GALOS Sample gc/ms unknown 11/3 Inst GC/MS Ins Mise ♦ Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Oxepane, 2,2,4-trimethyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 10.32 0.42 ng/uL 201434 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative/ID MW MolForm CAS# Qual

1 Oxepane, 2,2,4-trimethyl- 100 C6H120 023120-44-7 25 2 1-Butanol, 4-(1-methylethoxy) - 132 C7H1602 031600-69-8 12 3 Ether, 3-butenyl propyl 114 C7H140 034061-75-1 10 4 Oxirane, 2-methyl-3-propyl-, cis- 100 C6H120 006124-90-9 10 Abundance " Scan 597 (10.317 min): 26318.D (-) m/z 43.10 100.00% 43

5000 59

73 85 10.00 10.20 10.40 10.60 100 miz-> ........ -A + 4... 53.41 tH 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 T V m/z 59.10 46.04% Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 10.00 10.20 10.40 10.60 m/z 55.10 39.38% 31 85 100 Hmp Iummmasjup miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #5820:1-Butanol, 4-(1-methylethoxy)- 43 55 T T —A 10.00 10.20 10.40 10.60 73 m/z 41.10 34.96% 5000

89 60, 102 11 11 । i ! । i m 11 > i-rj-i > . i 11 > II 11 >. | i > 11 I I I I | I. .. 1111. ( I 11. . .. ].. . . । 11. ।. I. I । . . .. | I ... ।....,. mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 110 Abundance 43 #3059: Ether, 3-butenyl propyl 14 T ■ I —WA. —MA 10.00 10.20 10.40 10.60 m/z57.10 32.86% 5000

55 73 85 30 n/z-> — HT Tpagur 1’11111117 ... 11।. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 A.A n -A ‘ ' I 10.00 10.20 10.40 10.60

26318.D NP112701.M Tue Dec 04 10:12:43 2001 Page 3

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